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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 <br /> Job Number: C35685 <br /> Account: DECASM Dysert Environmental <br /> Project: Pactiv Packaging- 1110 Performance Drive Stockton CA 95206 <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> OP10684-MS Y27783.1) 1 09/03/14 MT 09/03/14 OP10684 EY1265 <br /> OP10684-MSD Y27784.1) 1 09/03/14 MT 09/03/14 OP10684 EY1265 <br /> C35683-1 Y27785.1) 1 09/03/14 MT 09/03/14 OP10684 EY1265 <br /> The QC reported here applies to the following samples: Method: SW846 8270C <br /> C35685-1 <br /> w <br /> C35683-1 Spike MS MS Spike MSD MSD Limits <br /> CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD <br /> 65-85-0 Benzoic acid ND 1660 955 57 1660 949 57 1 25-112/32 <br /> 95-57-8 2-Chlorophenol NO 832 404 49 831 360 43 12 31-110/31 <br /> 59-50-7 4-Chloro-3-methyl phenol ND 832 551 66 831 486 58 13 33-118/27 <br /> 120-83-2 2,4-Dichlorophenol ND 832 477 57 831 395 48 19 30-115/30 <br /> 105-67-9 2,4-Dimethylphenol ND 832 480 58 831 418 50 14 30-116/30 <br /> 51-28-5 2,4-Dinitrophenol ND 832 454 55 831 492 59 8 I1-139/30 <br /> 534-52-1 4,6-Dinitro-o-cresol ND 832 444 53 831 457 55 3 30-139/24 <br /> 95-48-7 2-Methylphenol ND 832 451 54 831 397 48 13 30-113/31 <br /> 3&4-Methylphenol ND 832 479 58 831 420 51 13 30-113/30 <br /> 88-75-5 2-Nitrophenol ND 832 391 47 831 334 40 16 29-112/32 <br /> 100-02-7 4-Nitrophenol ND 832 601 72 831 585 70 3 40-127/23 <br /> 87-86-5 Pentachlorophenol NO 832 600 72 831 591 71 2 43-140/20 <br /> 108-95-2 Phenol ND 832 450 54 831 407 49 10 30-112/30 <br /> 95-95-4 2,4,5-Trichlorophenol ND 832 555 67 831 469 56 17 33-121/27 <br /> 88-06-2 2,4,6-Trichlorophenol ND 832 502 60 831 406 49 21 31-115/29 <br /> 83-32-9 Acenaphthene ND 832 449 54 831 367 44 20 34-112/28 <br /> 208-96-8 Acenaphthylene ND 832 458 55 831 361 43 24 33-115/28 <br /> 62-53-3 Aniline NO 832 386 46 831 377 45 2 30-93/27 <br /> 120-12-7 Anthracene ND 832 563 68 831 547 66 3 59-111/21 <br /> 103-33-3 Azobenzene ND 832 511 61 831 449 54 13 39-114/22 <br /> 92-87-5 Benzidine ND 1660 ND 0*a 1660 174 10 200*a 10-96/39 <br /> 56-55-3 Benzo(a)anthracene NO 832 630 76 831 630 76 0 72-122/22 <br /> 50-32-8 Benzo(a)pyrene ND 832 602 72 831 596 72 1 71-120/22 <br /> 205-99-2 Benzo(b)fluoranthene ND 832 652 78 831 619 74 5 67-123/24 <br /> 191-24-2 Benzo(g,h,i)perylene NO 832 500 60 831 531 64 6 57-134/24 <br /> 207-08-9 Benzo(k)fluoranthene NO 832 612 74 831 642 77 5 74-126/25 <br /> 101-55-3 4-Bromophenylphenyl ether ND 832 547 66 831 481 58 13 45-110/22 <br /> 85-68-7 Butyl benzyl phthalate ND 832 656 79 831 700 84 6 68-129/20 <br /> 100-51-6 Benzyl Alcohol ND 832 465 56 831 411 49 12 25-116/31 <br /> 91-58-7 2-Chloronaphthalene ND 832 430 52 831 323 39 28 33-110/30 <br /> 106-47-8 4-Chloroani0ne ND 832 423 51 831 381 46 10 27-92/25 <br /> 86-74-8 Carbazole ND 832 628 75 831 602 72 4 64-125/21 <br /> 218-01-9 Chrysene NO 832 615 74 831 596 72* a 3 73-125/22 <br /> 111-91-1 bis(2-Chloroethoxy)methane ND 832 427 51 831 378 45 12 31-112/31 <br /> 111-44-4 bis(2-Chloroethyl)ether ND 832 361 43 831 313 38 14 30-106/31 <br /> 108-60-1 bis(2-Chloroisopropyl)ether NO 832 336 40 831 282 34 17 30-111/32 <br /> * = Outside of Control Limits. <br /> me 40 of 64 <br /> W ACCLJTEST. <br /> C35555 1..... — <br />