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l��-lti-lyyy t�tJ 5yF I`I t KUI'I TO 14252518782 P.07 <br /> HN3MM vERIZCATION LABORATORY ANALYSIS <br /> i <br /> TANK TANK TP1T-G TPH-D BTX & E CL HC TOTAL MTBE METALS <br /> CONTENTS 8015 8015 8020 8010 LEAD TBA, ICAP/ 827827 <br /> 826(0 8260 8260 ,8240 7420 DIPS0 <br /> Ff 2 AES or 8080 <br /> 7421 ETBg AA <br /> TAME <br /> 8260 <br /> LEADED GAS X X X X <br /> UNI,GAS X X X <br /> DIESEL X X <br /> 1 i <br /> KCFZOSENE X X <br /> UNK FUEL X X X X X <br /> -PROD_ OIL X X <br /> C40R. <br /> SOLVENTS X X <br /> i NONCHLOR <br /> SOLVENTS X X X <br /> i W,�STE\ <br /> USET?OIL X X X X X X <br /> UI analysts me ods art Idle design EPA metfzods descxtbed in EPA SW 846, 'Third Edition. 1 hose methods not found in <br /> ;WW spezificalN aored below. Refer to the 'SWRCB LUFT Field Manual", Appendix D(B), fable 3-5 on gage A20 for <br /> ainimu n dClea ion limits for rnmr vtiucle fuel(gasoline and diesel). Refer to 1-2-3 'Regional Board Staff R.ecommendarious <br /> or laitial val 'on arid'IuvesugatiOn of UST's" for the waste and motor oil minimum detection Urn <br /> )etection imi that imai'n below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> towever iabo Ory shall ua-Uac the Moet costive method. <br /> i <br /> i ° <br /> ABORAT TRY INALYM TERMWOLOG'y; <br /> PH-G I Tool Prxrolet=Hydrocarbon. Gasoline.GCIM(5030) 8015 mod or GC/MS 8260 <br /> PH-D TOW P=O(eum Hydrocarbon,Ditsd,GC/FID(3550).8015 mod or GCIMS 8260 <br /> TX&fi ,Tam.Xylene&Ethyl Benzene, GClPID 8020 or GC/MS 8260 <br /> L HC Chlorinated Hydrocir{,oa. GCIHSD 8010. GC/MS 8240 <br /> OTAL LEAD : TOW leo AA 7420, AA 7421 or 1CP-AES 6010 <br /> (TBE,TAkfE,DiPE.TBA . GC/MS 8260 <br /> OSTALS ICAP qr AA Induaive;Y Coed Plasma Anomic Emission Specavmeuy 6010 or Atomic Ahsorprion Spectromer y 7000_ <br /> J4etaL Cadmicaa, C IIMo tmm M=d VI. Lead,Zine sand Nickel. <br /> P0IYcWGri=1ed Biphenyls, GUMS 8270 or 8080 <br /> C-FID Gas Cb graphy.Flame Ionization Detection <br /> lediod 30SO Acid digestion <br /> `.edtod 350 Soxhlet sampk piepararion <br /> :ethod 3550 . Sonication sample ptepuation, exribciion method <br /> `ethodA/QC 5030 <br /> TQC Pkuge and trap sample Preparation <br /> Quality A=--cr./Quslity Control <br /> I <br /> rtes: To void alse positive derecuoa of b=zcne, benzene-free solvents are to be lewd. Fused capillary <br /> hunns; a�acke¢Colum ai ay be used as a "first cut- with-dirty'samples or once the hydrocarbons ha" bbeen characterized preferred <br /> and open <br /> A/QC is followed. proper <br /> )r dri king waref Sotures.P-EA recommends that the 500 series for volatile orgastic should be used in prcfcrenec to the 600 series because tlrc <br /> tection ligrits ark lower iad ri-le QA/QC is better. S"((!:s exhibiting arty [evcl of heavy metal coruamination ma <br /> iS--EUD tecomr�rends holding those r.m jcs until Y require ftuiAer analysis. <br /> disposal 15 lIIdlC3ttd_ <br /> 123 046 (RCVi led 10/19198) Page 8 <br />