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bL-ltd-lyyy er�:5yrr� rr<uri TO 14252518782 P.07 <br /> NfTNZMYJM VERMCAnON LABORATORY ANALXSIS <br /> i <br /> TANK , � 1 <br /> TANK TPH-G TPH-D BTX & E CL HC TOTAL MTBE ALS PCB <br /> CONTENT'S 8015 8015 8020 8010 LEAD TBA, [CAP/ 8270 <br /> ,gr.2 8260 8260 8240 7470 DIPE, AES or 8080 <br /> Ar 7421 EIRE, AA <br /> TAME <br /> 8260 <br /> L.81ADED GAS X I X X X I <br /> UNL GAS X X I X 1 <br /> DIESEL X X ( I <br /> KIosT✓xE x <br /> UNK FUEL X I X X I I X X <br /> I -PROD_ OILI <br /> X X <br /> CH40R. f <br /> i SOLVENTS X X I <br /> ! I <br /> I , <br /> SOLVENT'S X <br /> I X <br /> i <br /> WdSTE\ <br /> USP OIL x x x x X x <br /> VU an2iysis methods are the desip=d EPA methods des=lbxd in EPA SW=Third Fdition. T 0SC mcdhods not found in <br />;W 846 spe�iEcally aored below. Rafe;to the 'SWRCB LUPI'Fieid Manzlal', Append'u D (13 Table 3-1 on page A20 for <br /> ainimum dc=iou limits for motor vehicle fuel (gasoline and dial?). Refer to 1-2-3 ' <br /> Rtgional Board Staff Re�mmandatious <br /> or Initial Evac on and'Iuvessigaiion of T7ST"s' for the waste and motor oil minimum detecdon limits. <br />)election(L that t-emain below the MCL, STLC or Allowable Limit of the cotttamin= in question wiU be accepted, <br /> bwaver <br /> 1abon 10rY sh411 tmUze the most comervadve method <br /> i <br /> ABORATpRY ALYFZS TEFM OLOG'Y: <br /> PH_G I Toni e—_zm Hydroearom Gasoli=. GCiF D(5030) 8415 rood or GCIMS 8260 <br />?H-D ToW P=01etrm HydroartKm.Dksrf,GC/PID(3550), 8015 mod or GCIMS 8250 <br /> TX et E Barone, Toluaae,XY1me dt F.SttYl Bei GWID WM or GC/MS 8.260 <br /> L HC : Chlork=ed Hydromboa. GC41SD 8010. GCIMS 8240 <br /> OTAL LF AD Toml lead,AA 7420, AA 7421 or I01-AFS 6010 <br /> ME,TAYKE.DME.TBA . GC/MS 8260 <br /> MALS ICRP qr AA Inductively Coupled PUsma Momic Fmi joa Specavmer y 6010 or Atomic.absorption Spectrometry 7000- <br /> IJ Ham Cadmium,C rumi><mm M=4 w1. Lead, 71nc and Nickel. <br /> PofyCrlori=wd Biphcayts. GCW 8270 or 5080 <br /> C-FID Gas Chromatography. Fame Iottizatioa Detection <br /> lerhnd 3050 .kc zd digesuon <br />.CdWd 3541 Soxrler suupie ptvparawn <br /> sm <br />:eod 3550 . Sonication sample prrnr=on, ezu'acdon aimhod <br />"erhod 5030 Puuge and trap sample preparation <br /> AJQC I Quality ASsuran=JQtalrty Control <br /> I i <br /> xes: To avoid false positive der oa of bcazene. berzwso-free solve=am to be Itscd. Fused capWaty columns ate preferred to packed <br /> iumru; a�svice¢coluin�C=� y be¢sed as t 'first att' with "dirty'sarnplcs or ot>a the bydtvcarboas have bean chzrac.,csized and proper <br /> AJQC is followed. <br /> Ir dnalciug ware sourres.;E;?_4 recommends mat dse 500 s-ies for volatile organic should be used in pnfercn= to he of?0 se fes bemuse the <br /> coaion lirnics are lower ind die QAJQC is better. Samples ezhibKmg any level of iheivy m�conraminaci mat he 60u-e renes anslyse <br /> IS-I� tecomr�eads holding those=nples uml disposes! is indi=ed <br /> is- <br /> 123 046 (Pi:Yi fed to/1919g) Page 8 <br /> i <br /> • I <br />