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F K171 MCU�TOH -401f <br /> ENVO KO-TE(CHAnalytical Laboratory CERTIFICATE OF ANALYSIS <br /> Monday, June 2, 2008 <br /> Attention: Ryan Matthews <br /> Diamond Pet Foods Report Page 4 of 13 <br /> 250 East Roth Road <br /> Lathrop, CA 95330 <br /> Volatile Organic Compounds by EPA Method 8260B <br /> Sample Information <br /> Sample ID: Maint Shop Machine Tank Sample Type: Grab <br /> Laboratory ID: 8050709-01 Project Name: Coolant Waste Test <br /> Date/Time Sampled: 07-May-08 13:30 by Don Ngo Sample Matrix: Waste Water <br /> Test Parameter Resua DLR Unit Dilution Batch Prepared Analysis Date Method Notes <br /> Trichloroethene ND 0.500 ug/1 1 AE80705 07-May-08 07-May-08 EPA 82606 <br /> Trichlorofluoromethane ND 0.500 ug/I 1 AE80705 07-May-08 07-May-08 EPA 82608 <br /> ' 1,2,3-Trichloropropane ND 0.500 ug/I 1 AE80705 07-May-08 07-May-08 E <br /> _ _EPA 82606 <br /> 13,5-Tnmethylbenzene No 0.500 ug/I 1 AE80705 07-May-08 07-May-08 EPA 82608 <br /> 1 2,4-Trimethylbenzene ND 0.500 ug/l 1 AE80705 07-May-08 07-May-08 EPA 8260B <br /> Vinyl acetate ND 20.0 ug/I 1 AE80705 07-May-08 07-May-OB EPA 82608 <br /> Vinyl chloride No 0.500 ug/I 1 AE80705 07-May-08 07-May-08 EPA 82608 <br /> Methyl tertbutyl Ether(MtBE) ND 0.500 ug/I 1 AES0705 07-May-08 07-May-08 EPA 8260B <br /> m,p-Xylene ND 0.500 _ ug/I 1 AE80705 07-May-08 07-May-08 EPA-8-260B- <br /> Ethyl <br /> PA82608Ethyl Cert Butyl Ether(ETRE) ND 0.500 _ug/l 1 AE80705 07-May-08 07-May-08 EPA 82608 <br /> __. ._. _. __..---- <br /> _ ._—_ _. _____ ._ __ ____ ..__._ __ <br /> I tert-Amyl Methyl Ether(TAME) ND 0 500 _ug/I_ 1 _AE80705 07-May-08 07-May-08 EPA 82608 <br /> o-Xylene ND 0.500 ug/I _ _ 1 _ AE80705 07-May-08 07-May-08 EPA 82,508 <br /> tert-Butyl Acohol(TBA) ND 50.0 ug/I 1 AE80705 07-May-08 07-May-OB EPA 82608 <br /> Diisopropyl Ether(DIPE) _ ND0.500 ug/I 1 AE-807-05--07-May--08 07-May-08 EPA 82608 <br /> Su---- - _ _. _-_-- 100% 88-110 <br /> rrogete D 1uene-uorometbane 99% 86 118 <br /> SurrogateToluene-d8 _ <br /> Surrogafe:_4-BromoBuorobenzene 95% 86-115 - <br /> mg L--milligrams per liter ppm DLR=Defection limb for Purpose afReporung <br /> ug'l, -mmmgrams per Liter`ppb lisceptional sample matrices or interferences may <br /> result in higher detection limits. <br /> RESPECTFULLY SUBMITTED, <br /> Jonathan Le, Laboratory Director ' <br /> 3935 N. Coronado Ave. Stockton, CA 95204 Tel.: (209) 477-8105 Fax: (209) 546-7497 <br />