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���,• h 1534 Willow Pass Road,Pittsburg CA 94565-1701 <br /> McCampbell Analytical Inc. Toll Free Telephone:(877)252-9262/Fax(925)252-9269 <br /> "When Quality Counts" I http://w .mcc=pbeH.com/&nuil:nmin@mmampbeR.com <br /> Quality Control Report <br /> Client: C112MHELL WorkOrder: 1712687 <br /> Date Prepared: 12/18/17 BatchID: 150359 <br /> Date Analyzed: 12/18/17- 12/19/17 Extraction Method: SW5030B <br /> Instrument: GC10,GC28 Analytical Method: SW8260B <br /> Matrix: Soil Unit: mg/kg <br /> Project: 693815.TM.VA.01.00;PG&E 2017 Cntl Valley S- Sample ID: MB/LCS-150359 <br /> 600 MCDnldlslStn 1712761-OOIAMS/MSD <br /> QC Summary Report for SW8260B <br /> Analyte MS MSD SPK SPKRef MS MSD MS/MSD RPD RPD <br /> Result Result Val Val %REC %REC Limits Limit <br /> 1,1-Dichloropropene 0.0461 0.0429 0.050 NO 92 86 43-126 7.05 20 <br /> cis-1,3-Dichloropropene 0.0426 0.0407 0.050 NO 85 81 35-134 4.54 20 <br /> trans-1,3-Dichloropropene 0.0434 0.0422 0.050 NO 87 84 35-124 3.04 20 <br /> Diisopropyl ether(DIPE) 0.0438 0.0426 0.050 NO 88 85 49-116 2.78 20 <br /> Ethylbenzene 0.0513 0.0479 0.050 NO 103 96 49-137 6.99 20 <br /> Ethyl tert-butyl ether(ETBE) 0.0431 0.0421 0.050 NO 86 84 50-113 2.47 20 <br /> Freon 113 0.0425 0.0359 0.050 NO 85 72 28-114 16.9 20 <br /> Hexachlorobutadiene 0.0621 0.0592 0.050 NO 124 118 22-180 4.72 20 <br /> Hexachloroethane 0.0524 0.0502 0.050 NO 105 101 28-158 4.12 20 <br /> 2-Hexanone 0.0295 0.0301 0.050 NO 59 60 31-102 2.20 20 <br /> Isopropylbenzene 0.0620 0.0580 0.050 NO 124 116 50-153 6.62 20 <br /> 4-Isopropyl toluene 0.0627 0.0595 0.050 NO 125 119 41-171 5.34 20 <br /> Methyl-t-butyl ether(MTBE) 0.0438 0.0430 0.050 NO 88 86 48-110 2.04 20 <br /> Methylene chloride 0.0467 0.0441 0.050 NO 93 88 42-127 5.63 20 <br /> 4-Methyl-2-pentanone(MIBK) 0.0299 0.0297 0.050 NO 58 57 24-114 0.815 20 <br /> Naphthalene 0.0237 0.0236 0.050 NO 47 47 19-69 0 20 <br /> n-Propyl benzene 0.0612 0.0575 0.050 NO 122 115 46-168 6.21 20 <br /> Styrene 0.0524 0.0491 0.050 NO 97 90 42-122 6.38 20 <br /> 1,1,1,2-Tetrachloroethane 0.0432 0.0409 0.050 NO 86 82 52-121 5.52 20 <br /> 1,1,2,2-Tetrachloroethane 0.0376 0.0371 0.050 ND 75 74 27-116 1.36 20 <br /> Tetrachloroethene 0.0520 0.0477 0.050 NO 104 95 37-149 8.47 20 <br /> Toluene 0.0444 0.0411 0.050 NO 89 82 52-124 7.64 20 <br /> 1,2,3-Tdchlorobenzene 0.0296 0.0294 0.050 ND 59 59 20-86 0 20 <br /> 1,2,4-Trichlorobenzene 0.0390 0.0383 0.050 ND 78 77 24-107 1.71 20 <br /> 1,1,1-Trichloroethane 0.0480 0.0448 0.050 NO 96 90 48-128 7.02 20 <br /> 1,1,2-Trichloroethane 0.0419 0.0401 0.050 NO 84 80 51-110 4.43 20 <br /> Trichloroethene 0.0475 0.0456 0.050 NO 95 91 42-128 4.16 20 <br /> Trichlorofluoromethane 0.0450 0.0393 0.050 ND 90 79 31-121 13.7 20 <br /> 1,2,3-Tdchloropropane 0.0408 0.0408 0.050 NO 82 82 50-115 0 20 <br /> 1,2,4-Trimethylbenzene 0.0569 0.0542 0.050 NO 114 108 48-151 4.87 20 <br /> 1,3,5-Trimethylbenzene 0.0591 0.0560 0.050 ND 118 112 51-159 5.44 20 <br /> Vinyl Chloride 0.0428 0.0378 0.050 NO 86 76 11-136 12.2 20 <br /> Xylenes,Total 0.152 0.143 0.15 NO 101 95 38-141 6.22 20 <br /> : IX SEM® <br /> DEC 2 7 2017 <br /> (Cont.) <br /> CA ELAP 1644•NELAP 4033ORELAP ENVIRONMENTAL HEALTH <br /> DEPARTMENT Page 14 of 26 <br />