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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PC Boit 12425,Lancaster,PA 17605.2425•717-656-2300 Fax:717-8562681•www.lamwteriabs.com <br /> Page 6 of 6 <br /> Quality Control Summary <br /> Client Name: Secor International Group Number: 842784 <br /> Reported: 03/05/03 at 07:48 PM <br /> Surrogate Quality Control <br /> Limits: 80-120 60-120 81-117 74-121 <br /> Analysis Name: PPL + Xylene (total) by 8260 <br /> Batch number: K030572AB <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4001937 95 80 94 87 <br /> 4001938 97 85 10483 <br /> 4001940 97 83 97 86 <br /> Blank 99 91 96 90 <br /> LCS 99 88 102 96 <br /> MS 96 87 103 95 <br /> MSD 96 Be 101 95 <br /> Limits: 80-120 80-120 81-117 74-121 <br /> Analysis Name: PPL + Xylene (total) by 8260 <br /> Batch number: K030572AC <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-de 4-Bromofluorobenzene <br /> 4001931 96 83 99 92 <br /> 4001939 98 85 98 79 <br /> 4001941 97 64 102 84 <br /> Blank 94 87 97 93 <br /> LCS 99 88 102 96 <br /> MS 96 87 103 95 <br /> MSD 96 as 101 95 <br /> Limits: 80-120 80-120 81-117 74-121 <br /> e-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ. <br /> (2) The background result was more than four times the spike added. <br />