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bll""fINIUM VERIFICATION LABORATORY ANALYSIS <br /> TANK TANK TPH-G TFH-D BTX&E o"''GE-`ms <br /> X CONTENTS 8015 8015 $Ofo C TOTAL MTBE (MTBE. a¢rnss <br /> 8260 8260 8020 LEAD 8020 TBA,DIPE. ICAP/ PCB <br /> 8260 8240 7420 8260 ETRE. AES 8270 <br /> 8260 7421 TAME> or 8080 <br /> 8260 AA <br /> LEADED GAS X i <br /> X X X <br /> UNL GAS X X <br /> X <br /> DIESEL X X <br /> KEROSENE X X X <br /> UNK FUEL X X X <br /> X X <br /> PROD. OIL X X X <br /> CHLOR. <br /> SOLVENTS X X X <br /> NONCHLOR <br /> SOLVENTS X X X <br /> WASTEI <br /> USED OIL X X X X <br /> X X X <br /> All analysis methods are the designated EPA methods described in EPA SW 846, Third Edition. Those methods not found in SWWINNUM <br /> i 846 are specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix D(B),Table 3-5 on page A20 for <br /> minimum detection limits for motor vehicle fuel(gasoline and diesel). Refer to "Tri-Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's"for the waste and motor oil minimum detection limits. <br /> Detection Limits that remain below the MCL,STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon,Gasoline,GC/FID(50 )8015 mod r GC/MS 9260 <br /> TPH-D Total Petroleum Hydrocarbon <br /> ,Diesel.GC/FID(3550)30 8015 mod orGCIMS 8260 <br /> BTX&E Benzene,Toluene, Xylene&Ethyl Benzene,GC/PD)8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon,GC/HSD 8010.GGMS 8240 or 8260 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or ICP-AES 6010 <br /> OXYGENATES MTBE,ETRE,TAME,DIPE,&TBA GC/MS 8260(For MTBE screen only you may use 8020) <br /> Metals:Cadmium,Chromium III and VI,Lead,Zinc and Nickel. pecMETALS[CAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption S <br /> (tome try 7000. <br /> PCB Polychlorinated Biphenyls,GC/MS 8270 or 8080 <br /> GC-FID Gas Chromatography, Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlei sample preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of benzene, benzene-free solvents are to be used. Fused capillary columns are preferred to packed <br /> columns;a packed column may be used as a "first cut"with "dirty'samples or once the hydrocarbons have been characterized and proper <br /> QA/QC is followed. <br /> For drinking water sources,EPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the <br /> detection limits are lower and the QA/QC is beaer. Samples exhibiting any level of heavy metal comamination may require further analysts. <br /> PHS-EHD recommends holding those samples umtl disposal is indicated. <br /> EH 23 046 (Revised 05/09/00) Page 8 <br />