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I <br />I <br />INI <br />*ft., ..10, <br />one sample from beneath the tank is required. A short distance has been <br />defined by Region 2 Board engineers as not greater than twenty-four inches <br />below the backfill/native soil interface and is generally taken to be one <br />foot below the the backfill/native soil interface. This soil is brought up <br />in the backhoe bucket. A shovel or trowel is used to cut away surface soil <br />and backfill material which may have been included in the bucket, and the <br />sample is taken by pushing or driving a brass sample liner into the newly <br />exposed soil from the designated depth and location. Additional <br />clarifications by Region 2 Board engineers have indicated that when there is <br />an obvious difference in the relative contamination of soil brought up from <br />the interface depth, then it is the relatively more contaminated soil that <br />should be selected for inclusion in the sample. <br />ELECTIVE EXPLORATORY SAMPLES: This type of sampling employs the same <br />sample collection and handling procedures as are used in standard RWQCB <br />interface sampling, but soil is typically obtained at a greater depth or <br />from a position that is laterally offset from the interface location. <br />STOCKPILE SURVEY MODIFIED BAAQMD PROTOCOL: This sampling follows a <br />survey pattern, but uses a modified BAAQMD protocol for sampling stockpiles <br />of material that have been newly removed from a tank pit excavation. This <br />protocol calls for a discrete sample container to be collected for every 12.5 <br />cubic yards of material. The survey includes opposite sides of the <br />stockpile. Strict observance of the BAAQMD protocol (for purposes of <br />evaluating the levels of fuel vapor likely to be discharged from a stockpile) <br />calls for inclusion of the surface material in the brass liner which is <br />driven into the pile at a right angle (to the angle of repose) until the <br />liner is full. Unless specifically asked to follow the BAAQMD protocol, our <br />personnel routinely modify the procedure to exclude the surface soil and <br />collect soil from a depth of eight to eighteen inches. While this prejudices <br />the sample in the direction of ,yielding higher results than would a strict <br />BAAQMD sample, it is more representative of the levels of fuel hydrocarbons <br />present in the soil and is not likely to mislead the client or contractor <br />into offhauling or backfilling with soil stockpiles that are relatively clean <br />at the surface, but unacceptably contaminated through the remainder of their <br />volume. <br />SAMPLE CONTAINERS <br />C Our firm uses new sample containers of the type specified by either EPA or <br />the RWQCB for the collection of samples at sites where underground storage <br />tanks are involved. Water samples are contained in 40 ml volatile organic <br />analysis vials (VOAs) when analysis for gasoline and similar light volatile <br />compounds is intended. These containers are prepared according to EPA SW 846 <br />and will contain a small amount of preservative when the analysis is for TPH <br />as gasoline or EPA 602. Vials intended for EPA 601 analysis and EPA 624 GCMS <br />procedures are not preserved. Closure is accomplished with an open headed <br />(syringe accessible) plastic screw cap brought down on top of a Teflon faced <br />septum which is used to seal the sample without headspace. <br />Sampling Report 88280-M-1 CHEVRON 4054 page 10 <br />