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GeeAnalytical Laboratories; Inc. <br />1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br />Report # M333-32 <br />CERTIFICATE OF ANALYSIS Date: 12/04/01 <br />Date Rec'd: 11/29/01 <br />Wright Environmental Project: Joe Wilson Center-Tracy,CA Date Started: 12/03/01 <br />67 E 10th Street Date Completed: 12/04/01 <br />Tracy CA 95376 PO# Date Sampled: 11/29/01 <br />Time: <br />Sampler: R Azevedo (Geo) <br />Sample ID: Stock Pile South <br />Lab ID: M203765 <br />Method RL <br />Analyte <br />Results Units <br />8260B 5.0 <br />Benzene <br />ND pg/Kg <br />5.0 <br />Toluene <br />ND <br />5.0 <br />Ethyl Benzene <br />ND <br />5.0 <br />Total Xylenes <br />ND <br />10 <br />Methyl tert-butyl ether (MTBE) <br />ND <br />400 <br />Ethanol <br />ND <br />200 tert-Butanol <br />10 di -Isopropyl ether (DIPE) <br />10 Ethyl tert-butyl ether (ETRE) <br />10 tert-Amyl methyl ether (TAME) <br />Surrogate Amnt Spiked Amnt Recovered <br />1,2-Dichloroethane-d4 100 109 <br />2-Bmmo-l-chloropropane 100 85.9 <br />4'-Bromofluorobenzene 100 106 <br />Mario D'Ono <br />Chemist Certification # 1157 <br />ND <br />ND <br />ND <br />ND <br />Recovery <br />QC Limit % <br />109.0 <br />66-133 <br />85.9 <br />63-139 <br />106.0 <br />64-136 <br />Donna Keller <br />Laboratory Director <br />