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1534 <br /> 4;;S' <br /> McCampbell Analytical, Inc. www.m,low PassRoad,Pittsburg,CA 94565-1701 <br /> Web:www.mcwmphell.com E-mail:main(amccampbdl.com <br /> "When Ouelil Covets' Tele hme:877-252-9262 Fax:925-252-9269 <br /> ETIC Client Project ID: Sara Lee_Airport Date Sampled: 10/05/07 <br /> Date Received: 10/05/07 <br /> 2255 Morello Avenue <br /> Client Contact Marna Dougherty Date Extracted: I0/05/07 <br /> Pleasant Hill,CA 94523 Client P.O.: 62400145 Date Analyzed 10/06/07 <br /> TPH(g)&Volatile Organics by P&T and GC/MS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order: 0710257 <br /> Lab ID 0710257-002A <br /> Client ID PPS-2.5 <br /> Matrix Soil <br /> g Repmnng <br /> Compound Concentration* DF R-U.- <br /> ncenhation umo Compound Co " DF t.,m„ <br /> TPH ND 1.0 0.25 Acetone ND 1.0 0.05 <br /> Acrolein(Provenal) ND 1.0 0.05 A, lonitrile ND 1.0 0.02 <br /> Cert-Amyl methyl ether TAME ND 1. .005 Rer,em, ND 1.0 0,005 <br /> Bromobenzene ND 1.0 0.005 Bromochloromethane ND 1.0 0.005 <br /> Bromodicbloromethane ND 1.0 0.005 Bromoform ND 1.0 0.005 <br /> Bromomethane ND 1.0 0.0 2-Butanone MEK ND 1.0 0.02 <br /> t-But I alcohol TBA ND 1.0 0.05 n-Buryl benzene ND 1.0 0.005 <br /> sec-Butyl benzene ND 1.0 Q.005 tert-But I benzene ND 1.0 0.005 <br /> Carbon Disulfide ND 1.0 0.005 Carbon Tetrachloride ND 1.0 0.005 <br /> Chlorobemene ND 1.0 0.005 Chloroethane ND 1.0 10.005 <br /> 2-Chloroeth 1 Vinyl Ether ND 1.0 0.01 Chloroform ND 1.0 0.005 <br /> Chloromethane ND 1.0 0.005 2-Cblorotoluene ND 1.0 0.005 <br /> 4-Chlorotoluene ND 1.0 0.005 Dibromochloromethane ND 1.0 0.005 <br /> 12-Dibromo-3-chloro ro ane ND 1.0 0.00 1 2-Dibromoethane EDB ND I.0 0.005 <br /> Dibromomethane ND LO 0.005 12-Dichlorobenzene ND 1.0 0.005 <br /> 13-Dichlorobenzene ND 1.0 0. 0 1.4-Dichlorobenzene ND 1.0 0.005 <br /> Dichlorodifluoromethane ND 1.0 0.005 I 1-Dichloroethane ND LO 0.005 <br /> 12-Dichloroethane 12-DCA ND L0 0.005 11-Dichloroethene ND 1.0 0.005 <br /> cis-1 2-Dichloroethene ND 1.0 0.005 1 trans-1 2-Dichloroethene ND 1.0 0.005 <br /> 1 2-Dichloro ro ane ND 1.0 1 0.005 1 3-Dichloro ro ane ND 1.0 0.005 <br /> 2 2-Dichloro ro ane ND 1.0 0.005 1.1-Dichloroprovene ND 1 1.0 0.005 <br /> cis-1 3-Dichloro ro ene ND 1.0 0.005 trans-I 3-Dichloro ro ene ND 1.0 0.005 <br /> Diiso ro I ether DIPE ND 1.0 0.005 Ethanol ND 1.0 0.25 <br /> Eth (benzene ND 1.0 0.005 Ethyl ten-butyl ether ETBE ND 1.0 0.005 <br /> Freon 113 ND 1.0 0.1 Hexachlorobutadiene ND 1.0 0.005 <br /> Hexachloroethane ND 1.0 0.005 2-Hezanone ND 1.0 0.005 <br /> IsonronvIbenzene ND 1.0 0.005 4-Isopropyl toluene ND 1.0 0.005 <br /> Methanol ND 1.0 2.5 Meth I-t-but 1 ether MTBE ND L0 0.005 <br /> Meth l ne chloride ND 1.0 0.005 4-Meth I-2- entanone MIBK ND 1.0 0.005 <br /> Naphthalene ND 1.0 0.005 Nitrobenzene ND 1.0 1 0.1 <br /> n-Propyl benzene ND 1.0 0.005 Styrene ND 1.0 0.005 <br /> 1 1 1.2-Tetrachlorocthane ND 1.0 0,005 1 1 2 2-Telrachl roethane ND1.0 0.0 <br /> Tetra hloroethene ND 1.0 0.005 Toluene ND 1.0 0.005 <br /> l 2 3-Trichlorobenzene ND 1.0 0.005 1 2 4-Trichlorobenzene ND 1.00 <br /> .005 <br /> 1.1.1-Trichloroethane ND LO 0.005 112-Trichloroethane ND 1.0 0. 05 <br /> Trichloroethene ND 1.0 0.005 Trichlorofluoromethane ND 1.0 0.005 <br /> 1 2 3-Trichloro ro ane ND 1.0 1 0.005 1 1 2 4-Trimeth (benzene ND L0 0.005 <br /> 1 3 5-Trimeth (benzene ND 1.0 1 0.005 1 Vinyl Chloride ND 1.0 0.005 <br /> Surrogate Recoveries <br /> %SSI: 97 °/SS2: 96 <br /> Comments: <br /> °water and vapor samples are reported in pg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP extracts <br /> are reported in mg/L,wipe samples in pg/wipe. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or coelutes with another peak;&)low surrogate due to matrix interference. <br /> h)lighter than water immiscible sheen/product is present;it liquid sample that contains greater than-1 vol.%sediment;j)sample diluted due to high <br /> organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight;m) <br /> reporting limit raised due to insufficient sample amount;n)results are reported on a dry weight basis; )see attached narrative. <br /> DHS ELAP Certification No 1644 S Angela Rydelius,Lab Manager <br />