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DEU- U-y5 WEU 14:40 KLEINI•tLUEK l'HX NU, eWy 4buuel r loicu <br /> MIM,\ 1 VERIFIC.aT;UN LA30R-ATORY A,4.kLYF <br /> TANK ! TAINK I TPFi-G TPH-D BTX & E CL HC TOT.�i I KETALS PCB <br /> K CONTENTS 8015 3015 8020 3010 L.E. wrlA 1 ICA?/ 3270 <br /> 8:60 3260 3260 3240 74 0 702A I AES or 3030 <br /> 74 1 A4 <br /> LP 4DED X I :{ X <br /> GAS X <br /> UNL GAs I x X <br /> DIESEL X X I <br /> KEROSENE I X X <br /> UNK FUEL j X ( X X X <br /> PROD. OIL X x <br /> CHLOR. j <br /> so1.VEr'CS x <br /> NONcN?OR I j <br /> SOLVENTS x X x <br /> WASTE\ <br /> USED OCL x X X X k v <br /> All analyses methods are designated EPA methods described in EPA SW 3=6. Third Edition. Those methods not found <br /> in SW 3-L6, are specficaily noted below. Refer to the 'SWRCS LLF ?ield Manual', Appeadi. s-20, Table 3.5 for <br /> detection '.lints of motor vehicle fuels (gasoline and diesel). Refer to i-_ - 'Regional Board Staff Recammendaciorts for <br /> Initial Evaluation and investigation of U$T's" for the waste and motor oil detection limits. <br /> Detection Limits that remain below the MCL, ST—'C or Allowable Limit of the contaminant in question will he accepted, <br /> however laboratory shall utilize the most conSeiv2dye method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> rpH.G ora! Petroleum Hydtocrbon. Gasoline, GCFiD (5030) SOI: mad or GUMS 3250 <br /> TPH-D Total ?et:oleam F?ydrocnrbon, Diesel, GC/FiD (11550), 3015 mod or GC.-M5 3-60 <br /> 8TX & E Benzene, Toluene, Xylene & Ethyl Benzene, GCPID SC20 or GG1dS 3250 <br /> CL HC Chlorinated Hydrocarbor; GCIESD 3010, GCiVS 32?0 <br /> TOTAL LEAD Total lead, AA 742W, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide (DHS-AB :303), CG/61S 32;0 (DHS•LUF7 <br /> CC-FID Cas Chromatography, Flame Ionization Detection <br /> ICA? or A4 Inductively Coupled ?lasma Atomic Emission Soearomury 5010 or Atomic Absorption <br /> Spectrometry 7000. Metals: Cadmium, Chromium III and YT, Lead, Zinc and Nickel. <br /> PCB Polychlorinated Biphenyls, GQVS 82'0 or 3030 <br /> Method 3050 Ac d digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 5onication sample preparation- extraction method <br /> Method 5030 ?urge and trip sample preparation <br /> Q,VQC Quality Assurance/Quality Control <br /> Nota: To avoid false Oosidve detection of benzene, benzene-free solvents are to be used. Fused Capillary columns ase <br /> preferred to packed coiumns; a packed column may be used as a "first cuc' with "dirty' samples Or Once the hydrocarbons <br /> have been characterized and proper QA/AC is followed. <br /> For Drinking Hater sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br /> series because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heaLy metal <br /> contamination may re-ui:e further analysis. PHS-EiM recommends holding these samples unci disposal is indicted- <br /> EH 23 043 (Revised 7/10/W) Page 3 <br />