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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Phone (209) 572-0900 <br /> Modesto, CA 95351 FAX (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Oxygenates <br /> Report# K036-09 Date of Report: 02/11/99 <br /> Tuff Boy Trailers Date Received: 02/05/99 <br /> 5151 E.Almond Wood Ave. Date Started : 02/10/99 <br /> Manteca,CA. 95336 Date Sampled 02/05/99 Date Completed: 02/10/99 <br /> Sampler Ray Azevedo <br /> Project Name: Tank Removed by Thorpe Oil <br /> Sample ID: TK1 S @ 12' <br /> Lab ID: K20468 <br /> Method Detection Analyte Results Units <br /> Limit lAg/Kg <br /> 8260 250 Methyl tertiary-Butyl Ether (MTBE) ND <br /> 250 Ethanol ND <br /> 2500 tertiary-Butanol ND <br /> 250 Di-isopropyl ether (DIPE) ND <br /> 250 Ethyl tertiary-Butyl Ether (ETBE) ND <br /> 250 tertiary-Amyl Methyl Ether (TAME) ND <br /> Elevated detection limits due to the presence of heavier hydrocarbons. <br /> Sylvia Krenn Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />