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M MUM VERIFICATION LABORATORY, LYSIS
<br />All analyses methods are deaignatad IPA methods described in EPA SW 846, Third Edition. Those methods not found
<br />in SW 846, arespecifically noted below. Refer to the 'SV/RCB LUFr Field Manual', Appendix A-20, Table 3-5 for
<br />detealoe limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 'Regional Board Staff Recommendations for
<br />Initial &elnation and Investigation of USTY' for the waste and motor oil detection limits.
<br />DetecUm Umits that remain below tate MCI„ STLC or Allowable Undt of the eonta nhutat In question will be accepted,
<br />however laboratory shall utiixe the nowt cortser ratfse method.
<br />LABORATORY ANALYSES TERMINOLOGY:
<br />TPH-G
<br />Total Petroleum Hydrocarbon, Gasoline, ,GRID (5030) 8015 mod or CC/MS 8260
<br />TPH-D
<br />Total Petroleum Hydrocarbon, Diesel, GGPID (3550), 8015 mod or GCM 8260
<br />BTX do E
<br />Benzene, Toluene, Xylene dt Ethyl Beaune, GGPID 8020 or GCJMS 8M
<br />CL HC
<br />Chlorinated Hydrocarbon, GCAiSD 8010, GAMS 8240
<br />TOTAL LEAD
<br />Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />EDB
<br />Ethylene dibromide (DHS -AB 1803), GC1MS 8240 (DHS-LUFI)
<br />GC -FW
<br />Gas Chromatography, Flame Ionization Detection
<br />ICRP or AA
<br />Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption
<br />Spectrometry 7000. Metalm Cadmium, Chromium III and VI, Lead, Zinc and Nk*eL
<br />PCB
<br />Polychlorinated Biphenyh, GUMS 8270 or MW
<br />Method 3450
<br />Acid digestion
<br />Method 3540
<br />Soahlet sample preparation
<br />Method 3550
<br />Sonication sample preparation, extraction method
<br />Method 5030
<br />Parge and trap sample preparation
<br />QA/QC
<br />Quality AssuranceJQuality Control
<br />MEW
<br />a®aa��ae
<br />All analyses methods are deaignatad IPA methods described in EPA SW 846, Third Edition. Those methods not found
<br />in SW 846, arespecifically noted below. Refer to the 'SV/RCB LUFr Field Manual', Appendix A-20, Table 3-5 for
<br />detealoe limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 'Regional Board Staff Recommendations for
<br />Initial &elnation and Investigation of USTY' for the waste and motor oil detection limits.
<br />DetecUm Umits that remain below tate MCI„ STLC or Allowable Undt of the eonta nhutat In question will be accepted,
<br />however laboratory shall utiixe the nowt cortser ratfse method.
<br />LABORATORY ANALYSES TERMINOLOGY:
<br />TPH-G
<br />Total Petroleum Hydrocarbon, Gasoline, ,GRID (5030) 8015 mod or CC/MS 8260
<br />TPH-D
<br />Total Petroleum Hydrocarbon, Diesel, GGPID (3550), 8015 mod or GCM 8260
<br />BTX do E
<br />Benzene, Toluene, Xylene dt Ethyl Beaune, GGPID 8020 or GCJMS 8M
<br />CL HC
<br />Chlorinated Hydrocarbon, GCAiSD 8010, GAMS 8240
<br />TOTAL LEAD
<br />Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />EDB
<br />Ethylene dibromide (DHS -AB 1803), GC1MS 8240 (DHS-LUFI)
<br />GC -FW
<br />Gas Chromatography, Flame Ionization Detection
<br />ICRP or AA
<br />Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption
<br />Spectrometry 7000. Metalm Cadmium, Chromium III and VI, Lead, Zinc and Nk*eL
<br />PCB
<br />Polychlorinated Biphenyh, GUMS 8270 or MW
<br />Method 3450
<br />Acid digestion
<br />Method 3540
<br />Soahlet sample preparation
<br />Method 3550
<br />Sonication sample preparation, extraction method
<br />Method 5030
<br />Parge and trap sample preparation
<br />QA/QC
<br />Quality AssuranceJQuality Control
<br />Notes: To amid false positive detection of benzene, benzene -free solvents are to be used. Flued capillary columns ate
<br />preferred to packed columns; a packed column may be used as a 'first cut' with 'dirty' samples or once the hydrocarbons
<br />have been characterized and proper QA/AC is followed.
<br />For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600
<br />aeries because the detection limits are lower and the QA1QC Is better. Samples exhibiting any level of heavy metal
<br />contamination may require further analysis. PHS-EHD recommends holding these samples until disposal is indicated.
<br />EH 23 048 (Revised 7/10192) Page . 14
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