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y <br />..r <br />110 2nd Avenue South, #D7, Pacheco, CA 94553 <br />McCAMPBELL ANALYTICAL INC. Tele: 510-798-1620 Fax: 510-798-1622 <br />Upgradient Environmental <br />4111 82nd Street <br />Sacramento, Ca. 95682 <br />Client Project ID: # 94120; Alpine BP, <br />Stockton <br />Date Sampled: 09/14/94 <br />Date Received: 09/15/94 <br />Client Contact: Vic Cherven <br />Date Extracted: 09/21/94 <br />Client P.O: <br />Date Analyzed: 09/21/94 <br />LUFT Metals* <br />EPA analytical methods <br />239.2,6010` <br />213.1,6010 <br />218.1,6010 <br />249.1,6010 <br />289.1,6010 <br />Lab ID <br />Client ID <br />Matrix <br />Extraction° <br />Lead' <br />Cadmium* <br />Chromium <br />Nickel <br />Zinc* <br />41023 <br />Tank 4 @ 8' <br />S <br />TTLC <br />5.6 <br />ND <br />37 <br />42 <br />61 <br />41033 <br />Tank 4 Stockpile <br />S <br />TTLC <br />110 <br />ND <br />31 <br />27 <br />410 <br />Detection Limit unless otherwise <br />stated; ND means Not Detected <br />W <br />TTLC <br />0.005mg/L <br />0.01 <br />0.005 <br />0.01 <br />0.01 <br />S <br />TTLC <br />1.5mg/kg <br />0.5 <br />0.5 <br />0.5 <br />0.5 <br />—• <br />STLC,TCLP <br />0.20 mg1L <br />0.05 <br />0.02 <br />0.05 <br />0.05 <br />• soil samples are reported in mg/kg and water samples and all STLC & TCLP extracts in mg/L <br />+ Lead is analysed using EPA method 7420 (AA Flame)for soils, STLC & TCLP extracts and method 239.2 (AA Furnace) for water samples <br />o EPA waraction methods 1311(TCLP), 3010/3020(water,TT1,C), 3040(organic matrices,TTLC), 3050(solids,TTLC); STLC from CA Title <br />22 <br />a) liquid sample that contains greater than _ 2 vol. % sediments; the sediments are wdracted with the liquid, in accordance with EPA <br />methodologies and can significantly effect the metal's reported value. <br />DH S Certification No. 1644 f�i` Edward Hamilton, Lab Director <br />