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MCCAMPBELL ANALYTICAL INC. 110 2nd Avenue South, #D7, Pacheco, CA 94553 <br />Tele: 510-798-1620 Fax -510-798-1622 <br />Upgradient Environmental <br />4111 82nd Street <br />Sacramento, Ca. 95682 <br />Client Project ID: # 94120; Alpine BP, <br />Stockton <br />Date Sampled: 09/14/94 <br />Date Received: 09/15/94 <br />Client Contact: Vic Cherven <br />Date Extracted: 09/17/94 <br />Client P.O: <br />Date Analyzed: 09/17/94 <br />EPA method 601 or 8010 <br />Volatile Halocarbons <br />Lab ID <br />41023 <br />41033 <br />Client ID <br />Tank 4 8' <br />Tank 4 Stockpile <br />Matrix <br />S <br />S <br />Compound') <br />Concentration* <br />Concentration* Concentration* Concentration* <br />Bromodichloromethane <br />ND <br />ND <br />Bromoform(2) <br />ND <br />ND <br />Bromomethane <br />ND <br />ND <br />Carbon Tetrachloride(3) <br />ND <br />ND <br />Chlorobenzene <br />ND <br />ND <br />Chloroethane <br />ND <br />ND <br />2-Chloroeth l Yiny 1 Ether(e) <br />ND <br />ND <br />Chloroform (5) <br />ND <br />ND <br />Chloromethane <br />ND <br />ND <br />Dibromochlorotnethane <br />ND <br />ND <br />12 -Dichlorobenzene <br />ND <br />220 <br />13 -Dichlorobenzene <br />ND <br />15 <br />14 -Dichlorobenzene <br />ND <br />58 <br />Dichlorodifluoromethane <br />ND <br />ND <br />11-Dichloroethane <br />ND <br />ND <br />12-Dichloroethane <br />ND <br />ND <br />11-Dichloroethene <br />ND <br />ND <br />cis 12-Dichloroethene <br />ND <br />ND <br />trans 12-Dichloroethene <br />ND <br />ND <br />12-Dichloro ro ane <br />ND <br />ND <br />cis 13-Dichloro ro ene <br />ND <br />ND <br />trans 13-Dichloro ro ene <br />ND <br />ND <br />ethylene Chloride( <br />ND <br />ND <br />1,1,2.2 -Tetrachloroethane <br />ND <br />ND <br />Tetrachloroethene <br />ND <br />ND <br />111 -Trichloroethane <br />ND <br />t ND <br />1,1,2 -Trichloroethane <br />ND <br />ND <br />Trichloroethene <br />ND <br />ND <br />Trichlorofluoromethane <br />ND <br />ND <br />Vinyl Chloride() <br />ND <br />ND <br />% Recovery Surrogate <br />87 <br />88 <br />Comments <br />Detection limit unless otherwise stated: water, ND< 0.5u1/L; soil, ND< IOug/kg. <br />* water samples are reported in ug/L, soil samples in ug/kg and all TCLP extracts in ug/L <br />(1) IUPAC allows Vene" or "ene"; ex ethylene or ethene; (2) tribromomethane; (3) tetrachloromethane; (4) (2-chloroethoxy) ethene; (5) <br />trichlormethane dichloromethane chloroethene• 8 a lighter than water i nmiscible sbcen is present. <br />tiH5 L;ertlticatlOn NO. 1044 <br />i,' Edward Hamilton,Lab Director <br />