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Gea�!-tnalytical Laboratories;enc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> Report# P174-08 CERTIFICATE OF ANALYSIS Date: 6/26/03 <br /> Thorpe Oil Date Rec'd: 6/23/03 <br /> Date Started: 6/25/03 <br /> PO Box 357 Project: 767 N. Alpine Rd.-Stockton Date Completed:6/25/03 <br /> Lodi CA 95241 <br /> Date Sampled: 6/23/03 <br /> PO# Time: <br /> Sample ID: Stock Pile Sampler : R.Azevedo(Geo) <br /> Lab ID: P201084 <br /> Method RL Analyte Results Units <br /> 8260B 5.0 Benzene ND µg/Kg <br /> 5.0 Toluene ND <br /> 5.0 Ethyl Benzene ND <br /> 5.0 Total Xylenes ND <br /> 10 Methyl tert-butyl ether(MTBE) ND <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amot Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 20 23.4 117.0 66-133 <br /> 2-Bromo-l-chloropropane 20 22.1 110.5 63-139 <br /> 4-Bromofluorobenzene 20 20.2 101.0� y^.'t, 64-136 <br /> Q <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification#1157 Laboratory Director <br />