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110 2nd Avenue SouM%%7,Pacheco,CA 94553-5560 <br /> 4McCampbell Analytical, Inc. Tekphone:925-798-1620 Pax:925-798-1622 <br /> J Website:www.mccampbcll.com &mail:nninQtrccanpbell.com <br /> Shaw Environmental Client Project ID: #844915.74;SBC- Date Sampled: 09/16/04 <br /> Stockton <br /> 4005 Port Chicago Hwy Date Received: 09/16/04 <br /> Client Contact: Rob Debtagro Date Extracted: 09/16/04 <br /> Concord,CA 94520 <br /> Client P.O.: Date Analyzed: 09/16/04-09/17/04 <br /> Gasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline with BTEX and M'BE* <br /> Extraction rxthod: SPo'S030B Analyticalnethods: SW8021BI8015Cm Work Order. 0409242 <br /> Lab ID Client ID Matrix TPH(g) MTBE Benzene Toluene Ethylbenzene Xylenes <br /> r <br /> 001A CS-01-04 S -- -- ND ND ND ND 1 83.8 <br /> b. <br /> r <br /> r <br /> L <br /> L <br /> Reporting Limit for DF=1; W NA NA NA NA NA NA 1 ug/L <br /> ND means not detected at or <br /> r above the reporting limit S 1.0 0.05 0.005 0.005 1 0.005 1 0.005 1 1 n g <br /> •water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples in mg/kg, wipe samples in pg(vipe, <br /> pmduct/oil/non-aqueous liquid samples in mg/L. <br /> r <br /> #cluttered chromatogram;sample peak coelules with surrogate peak. <br /> +The following descriptions of the TPH chromatogram are cursory in nature and McCampbetl Analytical is not responsible for their interpretation:a) <br /> unmodified or weakly modified gasoline is significant;b)heavier gasoline range compounds are signi5cant(aged gasoline?);c)lighter gasoline range <br /> compounds(the most mobile fraction)are significant;d)gasoline range compounds having broad chromatographic peaks are significant;biologically <br /> altered gasoline?;e)TPH patten that does not appear to be derived from gasoline(stoddard solvent/mineral spirit?);f)one to a few isolated non-target <br /> peaks present;g)strongly aged gasoline or diesel range compounds are significant;h)lighter than water immiscible shem/product is present;i)liquid <br /> sample that contains greater than—1 vol.%sediment;j)reporting limit raised due to high MTBE content;k)TPH pattern that does not appear to be <br /> t. derived from gasoline aviation gas).m no recognizablepattern;n results are reported by dry weight <br /> DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />