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Nf*'.W:fUM VERIFICATION LABORATORY A`,06 ySIS <br /> TANK TAMC irH-G TPH-D BTX & E CL HC TOTAL ME'I'_.t,LS PCB <br /> # CONTENTS �t15 8015 8020 8010 LEAD t ICAP/ 5270 <br /> S_6) 8260 8260 8240 7420 AES or Soso <br /> 7421 AA <br /> LEADED <br /> GAS X X X <br /> Z UNL GAS X X <br /> DIESEL X X <br /> KEROSENE i X X <br /> UNK FUEL X X X X <br /> PROD. OIL X X <br /> CHLOR. <br /> SOLVENTS I X X <br /> NONCHLOR <br /> SOLVENTS X C X <br /> WASTE\ <br /> USED OIL X X X I X I x I X <br /> All analyses methods are desic-11ated EPA methods described in EPA SW 846, Third Edition. Those methods not found <br /> in SW 846, are specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix A-20, Table 3-5 for <br /> detection limits of motor vehicle rue's (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recom.m.endations for <br /> r. Initial Evaluation and Investiratioa of UST's" for the waste and motor oil detection limits. <br /> Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> r <br /> LABORATORY AAIALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline, GCFID (5030) 8015 mod or GC/MS S_60 <br /> TPH-D Total Petroleum Hydrocarbon, Diesel, GC ID (3550), 8015 mod or GC/MS S260 <br /> ` BTX & E Benzene, Toluene, Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 3260 <br /> CL HC Chlorinated Hydrocarbon, GCiHSD 8010, GGMS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethvlene dtbromide (DHS-AB 1303), GC/MS 8240 (DHS-LUFT) <br /> GC-FID Gas Chromatography, Flame Ionization Detection <br /> ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> .. Spectrometry 1000. Metals: Cadmium, Chromium III and V1, Lead, Zinc and Nickel. <br /> PCB Polychlorinated Biphenvls, GC/MS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of benzene, benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br /> ,. have been characterized and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br /> series because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br /> ` contamination may require further analysis. PHS-EHD recommends holding these samples until disposal is indicated. <br /> EH 23 048 (Revised 7/10/92) Page 8 <br />