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MINIf <br />M VGRIFICA"PION <br />I.ABORA'I'ORY <br />ANAL"�IS <br />v <br />TANK 1'PH-O <br />LFII -D <br />BTX & E <br />CL HC <br />TOTAL <br />MTBE <br />METALS <br />ICRP/ <br />PCB <br />8270 <br />TANK <br />CONTENTS 8015 <br />8015 <br />8020 <br />8010 <br />8240 <br />LEAD <br />742 <br />8020 <br />AES or <br />8080 <br />8260 <br />8260 <br />8260 <br />7420 <br />AA <br />LEADED <br />X <br />X <br />OAS X <br />UNL GAS X <br />X <br />DIESEL <br />X <br />X <br />j <br />KEROSENE <br />X <br />X <br />UNK FUEL X <br />X <br />X <br />X <br />PROD. OIL <br />X <br />X <br />CHLOR. <br />X <br />X <br />SOLVENTS <br />NONCHLOR <br />X <br />X <br />SOLVENTS <br />X <br />WASTE\ <br />USFD OIL X <br />X <br />X <br />X <br />X <br />X <br />cribed In EPA SW 846Third Edi <br />not <br />All analyses methods are designated EPA methods des, s <br />Appendix A-20, Table3-5 forund <br />in SW 846, are specifically noted below. Refer to the "SWRCB LUFI Field Manual", <br />defection limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for <br />Initial Evaluation and Investigation of UST's" for the waste and motor oil detection limits. <br />Beleclinn I.Imilq flint remain below the MCI„ STLC or Allowable Limit or the contaminant In question will be acceph d, <br />however laboratory shell utilize the most conservative method. <br />LABORATORY ANALYSES TERMINOLOGY: <br />TPII-O Total Petroleum Hydrocarbon, Gasoline, GClFID (5030) 8015 mod or ODMS 8260 <br />ITI1-D Total Petroleum Hydrocarbon, Diesel, GCJFID (3550), 8015 mod or GC/MS 8260 <br />BTX & E Benzene, Toluene, Xylene & Ethyl Benzene, OC/PID 8020 or GCIMS 8260 <br />CL HC Chlorinated Hydrocarbon, GGFISD 8010, GC/MS 8240 <br />TOTAL LEAD Total lead, AA 7420, AA 7421 or lCP-AES 6010 <br />EDB Ethylene dibromide (DIIS-AB 1803), GC/MS 8240 (DHS-LUFT) <br />GC -FID Gas Chrometogtaphy, Flame Ionization Detection <br />ICRP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br />Spectrometry 700. Metals! Cadmium', Chromium III and vi, Lead, Zine and Nickel. <br />CCB Polychlorinated Biphenyls, GC/MS 8270 or W80 <br />Method 3050 Acid digestion <br />Method 3540 Soxhlet sample preparation <br />Method 9550 Sonicalion sample preparation, extraction method <br />Method 5030 Purge and trap sample preparation <br />QA/QC Quality Assurance/Quality Control <br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns are <br />preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br />have been characterized and proper QA/AC is followed. <br />For Drinking water sources, EPA recommends that the 5W series for volatile organics be used in preference to the 600 <br />series because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br />contamination may require further analysis. PHS -121-11D recommends holding these samples until disposal Is indicated. <br />Ell 23 048 (RevlsedXJIMI) Page 8 <br />2/26/96 <br />