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GeoAnalytical Laboratories, Inc. <br />2300 Maryann Dr. Turlock CA 95380 Phone (209) 669.0100 Fax(209)668-8516 <br />email: lat.gm@att.net <br />Report# WOJ0706 Project: 8th & Eldorado Stockton Date: 10/14/10 <br />Jim Thorpe, Inc. Date Recd: 10/07/10 <br />PO Box 357 <br />Lodi, CA 95241 <br />Volatile Organic Chemistry - Quality Control <br />GeoAnalytical Laboratories, Inc. <br />Reporting Spike Source %RF,C RPD <br />knalyte Result Limit Units Level Result %REC Limits RPD _ Limit Notes <br />Batch W002752 - EPA 5030 Prepared & Analyzed: 10/11/10 <br />Blank (WO02752-BLKI) <br />1.2-Dichlomelhane <br />ND <br />5.D <br />ug/kg <br />Benzene <br />ND <br />5.0 <br />" <br />Di -isopropyl Edier(DIPE) <br />ND <br />10.0 <br />" <br />Ethanol <br />ND <br />400 <br />" <br />Ethyl tort -Butyl Ether(ETBE) <br />ND <br />10.0 <br />" <br />Ethylbenzene <br />ND <br />5.0 <br />" <br />Ethylene dibromide <br />ND <br />10.0 <br />" <br />Methyl ten -Butyl Ether(MTBE) <br />ND <br />10.0 <br />" <br />Tort -Amyl Methyl Eth"(TAME) <br />ND <br />10.0 <br />" <br />ten-Butaml(TBA) <br />ND <br />200 <br />" <br />Toluene <br />ND <br />5.0 <br />" <br />Xylenes, total <br />ND <br />5.0 <br />" <br />Gasoline <br />ND <br />1.0 <br />mgVkg <br />Surrogale.: 1,2-Drch1oroe1haned4 <br />19.5 <br />ug/kg <br />Woo <br />97 <br />72-132 <br />Surrogate: 2-Bry I-Chloropropane <br />11.1 <br />10.00 <br />106 <br />71-134 <br />Surrogate: 4-Bromofluorobeneene <br />19.6 <br />10.00 <br />98 <br />74-132 <br />Surrogate: 1,2-Dichloroethaned4 <br />0.0195 <br />mg/kg <br />D.02000 <br />97 <br />71-132 <br />Surrogate: 2-Bromo-l-Chloropropane <br />0.0211 <br />0.02001) <br />106 <br />71-134 <br />Surrogate:4-BnomoJluorobenzene <br />0.0196 <br />0.02000 <br />98 <br />74-132 <br />LCS(W002752-BSI) <br />_ _ <br />_ <br />_ -. <br />1.2-Dichloroethane <br />62.2 <br />5.0 <br />ug/kg <br />60.00 <br />104 <br />80-120 <br />Benzene <br />61.2 <br />5.0 <br />60.00 <br />102 <br />80-120 <br />Di -isopropyl Ether(DIPE) <br />57.9 <br />10.0 <br />60.00 <br />96 <br />80-120 <br />Methyl ten -Butyl Ether(MTBE) <br />60.6 <br />10.0 <br />60.00 <br />101 <br />80-120 <br />Tert-Amyl Methyl Ether(TAME) <br />58.0 <br />10.0 <br />60.00 <br />97 <br />80.120 <br />Toluene <br />52.9 <br />5.0 <br />60.00 <br />88 <br />80-120 <br />Gasoline <br />1.8 <br />1.0 <br />mg/kg <br />1.500 <br />117 <br />80-120 <br />Surrogate: 1,2-Drch1oroe1ham-d4 <br />12.1 <br />ug/kg <br />20,00 <br />110 <br />72-132 <br />Surrogate: 2-Bromo-1-Chloropropam <br />21.7 <br />20.00 <br />108 <br />71-134 <br />Surrogate: 4-BramoJluorobenaene <br />205 <br />20.00 <br />101 <br />74-132 <br />Surrogate: 1,2-Dichloroetharred4 <br />0.0215 <br />mglkg <br />0.02001 <br />107 <br />72-132 <br />Surrogate: 2-Bromo- l-Chloropropane <br />0.0200 <br />" <br />0.02000 <br />100 <br />71-134 <br />Surrogate: 4-8no a luorobenrene <br />0.0105 <br />0.02000 <br />102 <br />74-132 <br />Certification # 2585 <br />