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LABORATORY CONTROL SAMPLE DATA REPORT <br /> GC/MS Volatiles <br /> Client Lot #_ _ _ : E7B120147 Work Order #. . . : JPCWHIAC-LCS Matrix. . . . . . . . . .. SOLID <br /> LCS Lot-Sample#: E7B130000-223 JPCWHIAD-LCSD <br /> Prep Date. . . . . . : 02/12/07 Analysis Date. . : 02/12/07 <br /> Prep Batch #. . . : 7044223 Analysis Time. . : 15:08 <br /> Dilution Factor: 1 Instrument ID_ . : MSO <br /> Analyst ID. . . . . : 004648 <br /> SPIKE MEASURED PERCENT <br /> PARAMETER AMOUNT AMOUNT UNITS RECOVERY RPD METHOD <br /> Benzene 2500 2490 ug/kg 100 SW846 8260B <br /> 2500 2360 ug/kg 95 5.4 SW846 8260B <br /> Carbon tetrachloride 2500 2650 ug/kg 106 SW846 8260B <br /> 2500 2490 ug/kg 100 6.3 SW846 8260B <br /> Bromodichloromethane 2500 2900 ug/kg 116 SW846 8260B <br /> 2500 2760 ug/kg 110 5.0 SW846 8260B <br /> Chloroform 2500 2570 ug/kg 103 SW846 8260B <br /> 2500 2480 ug/kg 99 3.5 SW846 8260B <br /> 1,1-Dichloroethane 2500 2500 ug/kg 100 SW846 8260B <br /> 2500 2360 ug/kg 95 5.4 SW846 8260B <br /> 1,2-Dichloroethane 2500 2580 ug/kg 103 SW846 826013 <br /> 2500 2470 ug/kg 99 4.4 SW846 8260B <br /> 1,1-Dichloroethene 2500 2280 ug/kg 91 SW846 8260B <br /> 2500 2180 ug/kg 87 4.6 SW846 8260B <br /> cis-1,2-Dichloroethene 2500 2650 ug/kg 106 SW846 8260B <br /> 2500 2560 ug/kg 102 3.6 SW846 8260B <br /> Ethylbenzene 2500 2540 ug/kg 102 SW846 8260B <br /> 2500 2490 ug/kg 99 2.1 SW846 8260B <br /> Tetrachloroethene 2500 2490 ug/kg 100 SW846 8260B <br /> 2500 2440 ug/kg 97 2.3 SW846 826013 <br /> Toluene 2500 2440 ug/kg 98 SW846 8260B <br /> 2500 2380 ug/kg 95 2.5 SW846 8260B <br /> 1,1,1-Trichloroethane 2500 2700 ug/kg 108 SW846 8260B <br /> 2500 2590 ug/kg 104 4.2 SW846 8260B <br /> Trichloroethene 2500 2550 ug/kg 102 SW846 8260B <br /> 2500 2440 ug/kg 97 4.5 SW846 8260B <br /> Vinyl chloride 2500 2240 ug/kg 90 SW846 8260B <br /> 2500 2400 ug/kg 96 7.2 SW846 8260B <br /> m-Xylene & p-Xylene 5000 5130 ug/kg 103 SW846 8260B <br /> 5000 4980 ug/kg 100 2.9 SW846 8260B <br /> o-Xylene 2500 2530 ug/kg 101 SW846 8260B <br /> 2500 2470 ug/kg 99 2.4 SW846 8260B <br /> PERCENT RECOVERY <br /> SURROGATE RECOVERY LIMITS <br /> Bromofluorobenzene 103 (65 - 130) <br /> 90 (65 - 130) <br /> 1,2-Dichloroethane-d4 112 (65 - 130) <br /> 94 (65 - 130) <br /> Toluene-d8 106 (65 - 130) <br /> 91 (65 - 130) <br /> (Continued on next page) <br />