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MATRIX SPIKE. SAMPLE DATA REPORT TOTAL Metals Client Lot #. . . : E7B120147 Matrix. . . . . . . . . : SOLID Date Sampled. . . : 02/02/07 07:41 Date Received_ . : 02/02/07 16:30 SAMPLE SPIKE MEASRD PERCNT PREPARATION- WORK PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE ORDER # MS Lot-Sample #: E7B020351-001 Prep Batch #. . . : 7040299 8 Moisture. . . . . : 13 Cadmium ND 5.00 4.64 mg/kg 93 SW846 6010B 02/12-02/14/07 JNV811CT ND 5.00 3.97 N mg/kg 79 16 SW846 6010B 02/12-02/14/07 JNV811CU Dilution Factor: 1 Analysis Time. . : 21:15 Instrument ID. . : MO1 Analyst ID. . . ..: 021088 MS Run #..... . .: 7040170 Chromium 23.9 20.0 46.4 mg/kg 112 SW846 6010B 02/12-02/14/07 JNV811DJ 23.9 20.0 46.1 mg/kg 111 0.72 SW846 6010B 02/12-02/14/07 JNV811DK Dilution Factor: 1 Analysis Time..: 21:15 Instrument ID..: MO1 Analyst ID.. . ..: 021088 MS Run 4. ......: 7040170 Lead 10.4 50.0 61.1 mg/kg 101 SW846 6010B 02/12-02/14/07 JNV811CI 10.4 50.0 55.5 mg/kg 90 9.6 SW846 6010B 02/12-02/14/07 JNV8llC2 Dilution Factor: 1 Analysis Time..: 21:15 Instrument ID. . : MO1 Analyst ID... .. : 021088 MS Run #... . . . .: 7040170 Nickel 19.6 50.0 70.9 mg/kg 103 SW846 6010B 02/12-02/14/07 JNV8llC5 19.6 50.0 66.6 mg/kg 94 6.2 SW846 6010B 02/12-02/14/07 JNV811C6 Dilution Factor: 1 Analysis Time..: 21:15 Instrument ID..: 1401 Analyst ID. .. ..: 021088 MS Run #. . . ....: 7040170 Zinc 63.6 50.0 119 mg/kg 110 SW846 6010B 02/12-02/14/07 JNV81IDG 63.6 50.0 116 mg/kg 106 2.0 SW846 6010B 02/12-02/14/07 JNV811DH Dilution Factor: i Analysis Time.. : 21:15 Instrument ID. . : MO1 Analyst ID.. . . . : 021088 MS Run #. ...... : 7040170 NOTE(S) Calculations are performed before rounding to avoid round-off errors in calculated results. N Spiked analyte recovery is outside stated control limits.