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SAMPLING METHODOLOGIES USED ON THIS PROJECT STANDARD RWQCB INTERFACE SAMPLE: The tank removal sampling followed the standard protocol for obtaining interface samples. These samples fall into the category of samples which are known to be of primary concern to the interested regulatory agencies for determining if additional action will be required at a site and the methodology has been closely defined in state and RWQCB publications, supplements, and presentations. These specify both the acceptable depth and lateral situation of sample collection points. In accordance with these specifications, sample collection is executed as close as possible to the center line (longitudinal axis) of the tank and on a vertical axis with the fill pipe. A corresponding location is also found at the opposite end of the tank whenever standard interface samples are being collected. Briefly, the method consists of digging up native soil from directly below the fill pipe and the corresponding opposite end of the tank and obtaining a sample from the backfill/native soil interface or a short distance below the interface. In the case of tanks less than 1,000 gallons in capacity, only one sample from beneath the tank is required. A short distance has been defined by Region 2 Board engineers as not greater than twenty-four inches below the backfill/native soil interface and is generally taken to be one foot below the the backfill/native soil interface. This soil is brought up in the backhoe bucket. A shovel or trowel is used to cut away surface soil and backfill material which may have been included in the bucket, and the sample is taken by pushing or driving a brass sample liner into the newly exposed soil from the designated depth and location. Additional clarifications by Region 2 Board engineers have indicated that when there is an obvious difference in the relative contamination of soil brought up from the interface depth, then it is the relatively more contaminated soil that should be selected for inclusion in the sample. SAMPLE CONTAINERS Our firm uses new sample containers of the type specified by either EPA or the RWQCB for the collection of samples at sites where underground storage tanks are involved. Soil samples for volatile, semivolatile and nonvolatile analyses are all collected in properly prepared new brass liners which are 2 inches in diameter by 4 inches in length. Closure is accomplished with press fit plastic end caps which are fitted to the open ends of brass tube after a sheet of aluminum foil is wrapped over the exposed sample material. A non- contributing/nonsubtractive tape is wrapped completely around the joint areas where the plastic caps meet the outer wall of the brass tube. No preservative other than cold storage is used on samples captured in sample containers of this type. Sampling Report 88306-M-2 AL WILLIAMSON page 4