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A N A L T I C A L 1 <br /> 400, <br /> L LABORATORIES <br /> Rich Johnson Certificate of Analysis <br /> BSK and Associates - Sacramento Report Issue Date: 10/09/2000 <br /> 3140 Gold Camp Drive Suite 160 <br /> Rancho Cordova, CA 95670 <br /> BSK Submission #: 2000090726 <br /> BSK Sample ID#: 63004 <br /> Project ID: Project Desc: URSA Engineering <br /> Submission Comments: <br /> Sample Type: Solid Date Sampled: 09/20/2000 <br /> Sample Description: S-TE-10 Time Sampled: 1207 <br /> Sample Comments: Date Received: 09/21/2000 <br /> Inorganics Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> Cadmium(Cd) EPA 6010 ND mg/Kg I 1 1 10/03/2000 10/04/2000 <br /> Chromium-Total(Cr) EPA 6010 17 mg/Kg 5 1 5 10/03/2000 10/04/2000 <br /> Lead(Ph) EPA 6010 7.0 mg/Kg 5 1 5 10/03/2000 10/04/2000 <br /> Nickel(Ni) EPA 6010 16 mg/Kg 5 1 5 10/03/2000 10/04/2000 <br /> Zinc(Zn) EPA 6010 50 mg/Kg 5 1 5 10/03/2000 10/04/2000 <br /> Organics Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Diesel EPA 8015(M) ND mgfKg 2 1 2 10/02/2000 10/02/2000 <br /> TPH as Gasoline EPA 8015(M) ND mg/Kg 1 1 1 10/04/2000 10/04/2000 <br /> Arochlor 1016 EPA 8082 ND mg/Kg 0.1 1 0.1 09/26/2000 10/04/2000 <br /> Arochlor 1221 EPA 8082 ND mg(Kg 0.1 1 0.1 09/26/2000 10/04/2000 <br /> Arochlor 1232 EPA 8082 ND mg/Kg 0.1 1 0.1 09/26/2000 10/04/2000 <br /> Arochlor 1242 EPA 8082 ND mg/Kg 0.1 1 0.1 09/26/2000 10/04/2000 <br /> Arochlor 1248 EPA 8082 ND mg/Kg 0.1 1 0.1 09/26/2000 10/04/2000 <br /> Arochlor 1254 EPA 8082 ND mg/Kg 0.1 1 0.1 09/26/2000 10/04/2000 <br /> Arochlor 1260 EPA 8082 ND mg/Kg 0.1 1 0.1 09/26/2000 10/04/2000 <br /> 1,1,1,2-Tetrachloroethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> 1,1,1-Trichloroethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> 1,1,2,2-Tetrachloroethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> 1,1,2-Trichloroethane EPA 8260 ND pg(Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> 1,1-Dichloro-2-propanone EPA 8260 ND µg/Kg 25 1 25 10/01/2000 10/02/2000 <br /> ],I-Dichlormthane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> IJ-Dichloroethene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> l,l-Dichloropropene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> 1,2,3-Trichlorobenzene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> 1,2,3-Trichloropropme EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> 1,2,4-Trichlorobenzene EPA 8260 ND µg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> mg/L: Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H: Analyzed outside of hold time <br /> mg/Kg:Milligrams/Kilogram(ppm) DLR:Detection Limit for Reporting P: Preliminary result <br /> pg/L: Micrograms/Liter(ppb) :PQL x Dilution S: Suspect result. See Cover Letter for comments. <br /> pg/Kg: Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Rec:Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: IIIIIIIIIIININIIIIIIINIIIIIIIIIIIIIIIIIIIIIIRIIIIIIIIIIIIIINIIIIIIIII <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559485-6935 <br />