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A N A L Y T I C A L <br /> LABORATORIES <br /> Rich Johnson Certificate of Analysis <br /> BSK and Associates - Sacramento Report Issue Date: 10/09/2000 <br /> 3140 Gold Camp Drive Suite 160 <br /> Rancho Cordova, CA 95670 <br /> BSK Submission #: 2000090726 <br /> BSK Sample ID #: 63005 <br /> Project ID: Project Desc: URSA Engineering <br /> Submission Comments: <br /> Sample Type: Solid Date Sampled: 09/20/2000 <br /> Sample Description: S-TW-9 Time Sampled: 1200 <br /> Sample Comments: Date Received: 09/21/2000 <br /> Organics Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> Chloroform EPA 8260 ND gg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Chloromethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> cis-1.2-Dichloroethene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> cis-1,3-Dichloropropene EPA 8260 ND lig/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Dibromochloromethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Dibromomethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Dichlorodifluoromethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Diethyl ether EPA 8260 ND Vg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Di-isopropyl Ether EPA 8260 ND pg/Kg 20 1 20 10/04/2000 10/04/2000 <br /> Ethyl t-Butyl Ether EPA 8260 ND pg/Kg 20 1 20 10/04/2000 10/04/2000 <br /> Ethylbenzene EPA 8260 ND gg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Ethylmethacrylate EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Hexachlorobutadiene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Hexachloroethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> lodomethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Isopropylbenzene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> m,p-Xylenes EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Methylacrylate EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Methylene Chloride EPA 8260 ND vg/Kg 25 1 25 10/01/2000 10/02/2000 <br /> Methylmethacrylate EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Methyl-t-Butyl Ether EPA 8260 ND pg/Kg 20 1 20 10/04/2000 10/04/2000 <br /> Naphthalene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> n-Butylbenzene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Nitrobenzene EPA 8260 ND gg/Kg 25 1 25 10/01/2000 10/02/2000 <br /> n-Propylbenzene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> o-Xylene EPA 8260 ND pg/Kg 5.0 l 5 10/01/2000 10/02/2000 <br /> Pentachloroethane EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> p-Isopropyltoluene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> sec-Butylbenzene EPA 8260 ND pg/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> mg/L:Milligrams/Liter(ppm) PQL:Practical Quantitation Limit H:Analyzed outside of hold time <br /> mg/Kg: Milligrams/Kilogram(ppm) DLR: Detection Limit for Reporting P:Preliminary result <br /> pg/L: Micrograms/Liter(ppb) : PQL x Dilution S: Suspect result. See Cover Letter for comments. <br /> pg/Kg: Micrograms/Kilogram(ppb) ND:None Detected at DLR E:Analysis performed by External laboratory. <br /> %Rec: Percent Recovered(surrogates) See External Laboratory Report attachments. <br /> Report Authentication Code: 1111111111111111111111111111111111111111111111111111111111111111111111111 <br /> 1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935 <br />