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MA N A L Y�" T I C A L LABORATORIES QC Summary Report 10/10/2000 BSK Submission : 2000090726 Client: BSK and Associates-Sacramento Date Submitted 09/21/2000 Project ID: Project Dese : URSA Engineering BSK StarLims Run #: 12437 Analyte Results Matrix %Rec Spike Spk Matrix Analyte QC Typ, Spike ID Result Units or RPD RPD Cone Cone UCL LCL Date Cadmium(Cd) LCS N/A 25.3 mg/Kg 101 25 ND 130 70 10/04/00 Acceptable Chromium-Total(Cr) LCS N/A 100 mg/Kg 100 too ND 130 70 10/04/00 Acceptable Lead(Ph) LCS N/A 201 mg/Kg 100 200 ND 130 70 10/04/00 Acceptable Nickel(Ni) LCS N/A 106 mg/Kg 106 100 ND 130 70 10/04/00 Acceptable Zinc(Zn) LCS N/A 98.4 mg/Kg 98 100 ND 130 70 10/04/00 Acceptable Cadmium(Cd) LCSD N/A 25.7 mg/Kg 102 1.6 25 ND 130 70 10/04/00 Acceptable Chromium-Total(Cr) LCSD N/A 100 mg/Kg 100 0.0 100 ND 130 70 10/04/00 Acceptable Lead(Ph) LCSD N/A 197 mg/Kg 98 2 200 ND 130 70 10/04/00 Acceptable Nickel(Ni) LCSD N/A 105 mg/Kg 105 0.95 100 ND 130 70 10/04/00 Acceptable Zinc(Zn) LCSD N/A 99.5 mg/Kg 98 0.1 100 ND 130 70 10/04/00 Acceptable Cadmium(Cd) MS 63004 25.2 mg/Kg 100 25 ND 130 70 10/04/00 Acceptable Chromium-Total(Cr) MS 63004 113 mg/Kg 96 too 17 130 70 10/04/00 Acceptable Lead(Ph) MS 63004 196 mg/Kg 94 200 7.0 130 70 10/04/00 Acceptable Nickel(Ni) MS 63004 113 mg/Kg 97 100 16 130 70 10/04/00 Acceptable Zinc(Zn) MS 63004 145 mg/Kg 96 100 50 130 70 10/04/00 Acceptable Cadmium(Cd) MSD 63004 25.3 mg/Kg 101 0.39 25 ND 130 70 10/04/00 Acceptable Chromium-Total(Cr) MSD 63004 112 mg/Kg 95 0.89 too 17 130 70 10/04/00 Acceptable Lead(Pb) MSD 63004 195 mg/Kg 94 0.52 200 7.0 130 70 10/04/00 Acceptable Nickel(Ni) MSD 63004 115 mg/Kg 99 1.8 loo 16 130 70 10/04/00 Acceptable Zinc(Zn) MSD 63004 144 mg/Kg 96 0.7 100 50 130 70 10/04/00 Acceptable Cadmium(Cd) RBLK N/A 0 mg/Kg <1 1 N/A 10/04/00 Acceptable Chromium-Total(Cr) RBLK N/A 0 mg/Kg <5 5 N/A 10/04/00 Acceptable Lead(Ph) RBLK N/A 0 mg/Kg <5 5 N/A 10/04/00 Acceptable Nickel(Ni) RBLK N/A 0 mg/Kg <5 5 N/A 10/04/00 Acceptable Zinc(Zn) RBLK N/A 0 mg/Kg <5 5 N/A 10/04/00 Acceptable BSK StarLims Run #: 12439 Analyte Results Matrix %Rec Spike Spk Matrix Analyte QC Type Spike Ill Result Units or RPD RPD Cone Cone UCL LCL Date 1,2-Uibromoethane LCS N/A 12.84 pg/L 102 12.5 ND 130 70 10/04/00 Acceptable 1,2-Dichloroethane LCS N/A 12.65 pg/L 101 12.5 ND 130 70 10/04/00 Acceptable Di-isopropyl Ether LCS N/A 13.35 pg/L 106 12.5 ND 130 70 10/04/00 Acceptable %Rec: Percent Recovered Parent Sample: Sample used as background matrix for MS/MSD Page 6 of 8 RPD: Relative Percent Difference 0()S-High: QC Result Above UCL UCL: Upper Control Limit OOS-Low: QC Result Below LCL LCL: Lower Control Limit