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10/09/00 MON 19:09 FAX 9168539297 BSK Sacramento Z009 <br /> 10/06/2000 FRI 14:44 FAX 559 4es 6033 BSK LAIIS C�jD10/013 <br /> ,ser <br /> A N A L Y T I C A L <br /> L■Z`1il LABORATORIES <br /> Rich Johnson Certificate of Analysis <br /> BSK and Associates - Sacramento Report Issue Date: 10/0620DO <br /> 3140 Gold Camp Drive Suite 160 <br /> Rawubo Cordova, CA 956.10 <br /> BSK Submission N: 2000090726 <br /> BSK Sample ID N: 63010 <br /> Project m: Project Desc: URSA Eaglaee m6 <br /> submi"we comsocuu: <br /> sample Typo: Solid hate sampled: 0920/2000 <br /> Samplc Description: Compovi[e SamDles S-CMPI-S-CMP4 Time Sampled: 1207 <br /> Sample Comments: tete Received: 09212000 <br /> borganics Prep &made <br /> Analyte Method Result Unita rQL Dilution DLR Date Date <br /> Cadmium(Cd) LPA 6010 NO mg/Kg 1 1 i 10/032000 10/04/2000 <br /> utvom=-Total(Cr) F:PA6010 17 mg/1Cg 5 1 J 10/032000 10/042000 <br /> Lasd(PI,) GPA 601D 5.0 Mg/Kg 5 I 5 10/052000 10/04/2000 <br /> Nickel(Ni) EPA6010 16 ms%g 5 1 5 10/032000 10/042000 <br /> Ziac(7a) SPA6010 30 mgT4 5 1 5 10/032000 1/011420(10 <br /> Organics Prep Anstysis <br /> Analyte Method Result Units PQL DDution DLR Date Date <br /> TPI1 os Diesel r'.PA8015(h1) 2.4 mg/Kg 2 1 2 lo/02/2000 101032000 <br /> TP11 as Gasdnw HPA 901 5M ND nwKg 1 1 1 10/032000 10/0312000 <br /> Arochlor 1016 EPA 8082 NO M&gcg 0,1 1 0.1 D9262000 10/04/2000 <br /> Axwhlor 1221 EPA 30a2 Nn maOto 0.1 I 0.1 AOnA/20M l0/04M00 <br /> A-ocblor 1232 EPA 9082 NO mg/Kg 0.1 1 0.1 0926/2000 10/04/2000 <br /> Arncblor 1242 EPA 8082 NO m&IKg 0.1 1 0.1 09262000 1010412000 <br /> Aroehlor 124E EPA 9082 NO mrj'Kg 0.1 l 0.1 09/26/2000 1/004/2000 <br /> Arcohlor 1254 EPA 8082 NO mg/Kg 0.1 1 0.1 09262000 10104:2000 <br /> Arachlor 1260 KrA 6042 NO n*Kg 0.1 t 0.1 0Y/2b/2(1t1U IW0412W0 <br /> 1,1,1,2-fetrxhloloetbane EPA 9260 NO N&xg $.0 1 5 10/012000 10/022000 <br /> I,I,1=fdchleroabane <br /> RPA U,60 NO µr/Kg 5.0 1 5 10/012000 1W)W2000 <br /> 1.122+r�oo:Wu,cJwn: "A aroma rvaa i•eavo <br /> 1,1,2-Trichlcroulww EPA 8260 NO µg/Kg 5.0 1 5 10/01/2000 10;02/2000 <br /> l,t-Dlchloro-2-propmonc EPA 9260 Nn µ8/K8 25 1 25 10/01/2000 10/022000 <br /> 1,14Dichloroetllme CPA 8260 ND Pg/4 5.0 1 5 LO/01/2000 10/022000 <br /> I,l-Dichbroelbeec EPA 8260 NO ).du 5.0 1 5 10/012000 101022D00 <br /> 1,1-Didilaomopcnc UA:3260 ND 11" 5.0 1 5 10/012000 10/022000 <br /> 1.2.3-Tricblombca m FPA 8260 ND µ8/K8 5.0 1 5 10/0120DO 1 D/022000 <br /> 1,2,3=1'ricNoropropam FPA 9260 ND µg/Kg 5.0 1 5 10/012000 tNomwo <br /> ',,Z,t'rriahlorohcaecac <br /> PPA 8200 NO µy/Ag <br /> S_0 1 • 10/012000 t0/022000 <br /> mA L:milligw whiter(ppm) PQL:practical quantitation limit H:analy?cd Dutsids of hold time <br /> mg/Kg-millierams4cilogram(ppm, DLR:det=tiou limit for reporting P:prclimmary rerun <br /> µ8/L:micrograrowliter(ppb) :PQL x Dilutoa S:suspect result. See Cover Lew for cocr a is <br /> µg/.Kg:micrograms/kilogram(ppb) NO:none ddccttd at DLR <br /> /Rev percent recovered(Amptcs) <br />