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10!09,,00 NON 13:05 PAX 9168539297 BSK Sacramento ®011 <br /> 10/06/2000 FRI 17: 85 FAX 559 ,..^a5 6933 BSK LABS Q012/013 <br /> A N A L Y T I C A L <br /> LABORATORIES <br /> Rich Johnson Certificate of Analysis <br /> BSK and Associates - Sacrunento Report Issue Date: 10/062000 <br /> 3140 Gold Camp Drive Suite 160 <br /> Rancho Cordova, CA 95670 <br /> BW Submission#: 2000090926 <br /> BSK Sampk TD#: 63070 <br /> Pr%Rl m: Project Dese: URSA Engineering <br /> Submbsion Co-=Ls: <br /> Sample Type: Solid Dau Ra npled: 09,202000 <br /> Sample Dceviption: COmpOaite Samples S-CMPI-S-CMP4 Time Sampled: 1207 <br /> Sample Comments: Date Received: 09212000 <br /> Organics <br /> Prep Analysis <br /> Analyze Method Resuk Umib PQL Dilution DLR We Date <br /> ublorotmm EPA 8260 ND µ&/ICI, $.0 1 5 I0/01/2(1(10 10/02/2000 <br /> CblommetMne FPA 8260 ND µ&/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> cu-12-Dia6oroedKne EPA 8260 ND µg%g; 5.0 1 5 10/01/2000 10H12/2000 <br /> cwt.Wichloropropene EPA8260 ND µgag 5.0 1 5 10/01/2000 11/022000 <br /> [AhnXra4WQroMelNarle EVA 1260 ND pg]Kg 5.0 1 5 IO/U1/20(10 lutflly200U <br /> Dibromomcdunc EPA 8260 ND pg/Kg 5-0 1 5 10/01/2000 10/02/2000 <br /> Dicldoroditluoromcdaurc EPA 8260 NO µ&/Kg 5.0 1 5 10/01/2000 10102/2000 <br /> Diclhyl ethm EPA 8260 ND µ&/Kg 5.0 1 5 10/01/2000 10/02/2000 <br /> Di-(wlxopyl Ether EPA 8260 ND µ&/Kg 20 1 20 10/04/2000 10iO42000 <br /> Ethyl t-Baty!Elba EPA 8260 ND µ&/Kg 20 1 20 10/04/2000 l IV04/2000 <br /> my1Lc.a w CPA 6260 ND µ&/Kg 5.0 1 5 10101/2000 10/02/2000 <br /> FAhylmcthaorylarc EPA 8260 Nn 1rP/K6 50 1 S 10/01/2011 11/(12/20011 <br /> Hczachlorobutadiene EVA 8260 No pg/Kg 5.0 1 5 10/o1/2000 10/022000 <br /> He wwwocNaac EPA 8260 ND pp/Kg 5.0 1 5 10/01/50M 10/022000 <br /> loinmethenc EPA 8260 ND pg/K& 5.0 1 5 10/012000 10,,022000 <br /> Isopropylbcnzmc EPA 8260 ND µg/Kg 5,0 1 5 10/01/2000 10/02/2000 <br /> u1P-Xylcnes EPA 8260 ND µ&/Kg 5.0 1 5 10/012000 1Di022000 <br /> M.Npls<yla. L-r+A 5340 ND µyrcg 5.0 1 S 10/01/5000 W/01,3000 <br /> MrftIMP(TlnriAw FOA 11" ND I-afga 7q 1 2f Inin1/2nr11 Inw,iwn <br /> Methylmedzacrylate EPA 8260 ND p&/Kg 5.0 1 5 l0/01/20W IW022000 <br /> Methykaln(yl Ether EPA 8260 ND µ&/Kg 10 1 10 10/012000 10!02/2000 <br /> Mothyk-Butyl Ether PP 8260 ND pg/Kg 20 1 20 10/04n0(M I NW2000 <br /> Naphiaiune m'A BLbu ND pg/Kg ).0 1 5 IWUI/2WU IuluzILuuu <br /> B.tylhamono CTA 926A ND pg/Kg 5.0 1 5 10/01/2000 I W0212000 <br /> Nlnobenzenc EPA 8260 ND µ&/Kg 2$ 1 25 10/01/2000 10/022000 <br /> u-Propylbeamne EPA 8260 ND µ&/Kg 5.0 1 5 10/01/2000 10!022000 <br /> o-Xylene EPA 6260 ND µµ/Kg 5.0 1 5 10/01/2000 10/022000 <br /> Pcntnworoethnne EPA 8260 ND pg/Kg 5.0 1 5 10/01PLO00 IW022000 <br /> P-tsoproPylnol.unc EVA 8260 ND pg/Kg 5.0 l 5 10/01/2000 10/02/2000 <br /> Mgr7.:milli&e0s/111e(PPM) ML:pmcti al qumfitatlon limit tI:analyzed outside of hold time <br /> mg/Kg:milbWams/kilogrm(Ppm; DLR:dczectlo0 limit for reporting P:preliminary result <br /> µ%A,:miarognadlitor(ppb) :POL x Dilution. S:mspoct mutt. Sec Cover Lanes for couuorns <br /> µ&/Kg:micrognau vIcalograrn(ppb) M):none detected ml DLR <br /> %R=percent recovered(-surrogates) <br />