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03/19/2002 10: 53 5720916 GEOANALYTICAL LAB PAGE 02 <br /> v <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> ReportM M355-20 Date: 12/27/01 <br /> Thome Oil Project: Mosquito Abatement- Re-Sample Date Reed: 12/21/01 <br /> PO Box 357 Date Started: 12/26/01 <br /> Lodi CA 95241P0# Date Completed: 12/27/01 <br /> Date Sampled: 12/21/01 <br /> Sampler: RAzevedo(Geo) <br /> Sample ID Lab ID RL Method An Results Unita <br /> TKl-East ® 13' 12/21/01 M203992 5.0 8021B Benzene ND pg/Kg <br /> 5.0 Toluene ND pg/Kg <br /> 5.0 Ethyl Benzene ND N8/4 <br /> 5.0 Total Xylenes ND P9/1(9 <br /> 10 Methyl tent-Butyl Ether ND PVKg <br /> Surtopte A=t Spiced Amnt Rec. %Recovery QC Limit% <br /> a,a,a-TFT 250 208 83.2 66-117 <br /> Stock Pile 12/21/01 M203993 5.0 8021E Benzene ND / <br /> 5.0 Toluene <br /> IVP p8/K8 <br /> 5.0 <br /> Ethyl Benzene ND / <br /> 5.0 lg <br /> Total Xylenes ND pg/Kg <br /> 10 Methyl tert-Butyl Ether ND }t$/Kg <br /> Su—p a Aautr Spiked Aunt Rec. %Recovery QC Limit% <br /> apa-TFr 250 273 109-2 66-117 <br /> 41 <br /> Mario D'Onofno Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />