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&— Sequoia <br />Analytical <br />*401e <br />NVIII10 <br />Sampled: 10/09/96 <br />270 Perkins Ave. <br />680 Chesapeake Drive <br />Redwood City, CA 94063 <br />(415) 364-9600 <br />FAX (415) 364-9233 <br />404 N. Wiget Lane <br />Walnut Creek, CA 94598 <br />(510) 988-9600 <br />FAX (510) 988-9673 <br />819 Striker Avenue, Suite 8 <br />Sacramento, CA 95834 <br />(916) 921-9600 <br />FAX (916) 921 .0 IGO <br />... . ........... . ......... . ............ . ........ . . . <br />Enviros <br />Client Pro'. ID: Shell 3011 Benjamin Holt Dr. <br />Sampled: 10/09/96 <br />270 Perkins Ave. <br />Sample Descript: ST -5 <br />Received: 10/09/96 <br />Sonoma, CA 95476 <br />Matrix: SOLID <br />Extracted: 10/09/96 <br />Analysis Method: 8015Mod/8020 <br />Analyzed: 10/10/96 M <br />Attention: Joe Neely MMUN <br />ry -2:23 <br />Lab Number: 9610568-05 -MMMUMUMM.M. <br />MN .. ...... . ....... . ........... <br />......... . .... .............. ....... ............. . ... ....... ... <br />R n <br />Nt .............. . ........ . ... 'MUM1111M.NNIM. —13 <br />nanum .MUN-UMN.-aaaaam ii <br />......... . .. . .. . .......... <br />. .... ....... . an- <br />)C Batch Number: GC100996BTEXER§ <br />imsm! . <br />as:::: ................. <br />is: mmm 33: <br />=MMUMM <br />............................. 1. a,.:,aRMs <br />istrument ID: GCHP06 <br />Total Purgeable <br />Petroleum Hydrocarbons (TPPH) with BTEX and IIVITBIE <br />Analyte <br />Detection Limit <br />Sample Results <br />mg/Kg <br />mg/Kg <br />TPPH as Gas <br />.................... 1.0 <br />.................... 4.9 <br />Methyl t -Butyl Ether <br />.................... 0.025 <br />.................... 1.1 <br />Benzene <br />.................... 0.0050 <br />.................... 0.0096 <br />Toluene <br />0.0050 <br />N.D. <br />Ethyl Benzene <br />.................... 0.0050 <br />.................... 0.015 <br />Xylenes; (Total) <br />.................... 0.0050 <br />.................... 0.046 <br />Chromatogram Pattern: <br />.................... <br />.................... C6 -C12 <br />Surrogates <br />Control Limits % <br />% Recovery <br />Trffluorotoluene <br />70 <br />130 82 <br />Analytes reported as N.D. were not present above the stated limit of detection. <br />SEQUOIA ANALYTICAL - ELAP #1210 <br />za� <br />Mike"Gregory <br />Project Manager <br />Page: 7 <br />