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Sequoia <br />Analytical <br />270 Perkins Ave. <br />Sonoma, CA 95476 <br />Instrument ID: <br />Analyte <br />TPPH as Gas <br />Benzene <br />Toluene <br />Ethyl Benzene <br />Xylenes (Total) <br />Chromatogram Pattern: <br />Surrogates <br />TriFluorotoluene <br />680 Chesapeake Drive Redwood City, CA 940%0 (415) 364-9600 FAX (415) 364.9233 <br />404 N. Wiget lane Walnut Creek, CA 94598 (510) 988-9600 FAX (510) 988.9673 <br />819 Striker Avenue, Suite 8 Sacramento, CA 95834 (916) 921-9600 FAX (916) 92 1 -0 100 <br />Proj. ID: Shell 3011 Benj; <br />e Descript: SS4C <br />: SOLID <br />;is Method: 8015Mod/8020 <br />Extracted: <br />Analyzed: <br />Total Purgeable Petroleum Hydrocarbons (TPPH) with BTEX <br />Detection Limit <br />mg/Kg <br />.................... 2.0 ................. <br />0.010 <br />0 010 <br />Sample Results <br />mg/Kg <br />.................... 0.010 .................... <br />.................... 0.010 .................... <br />.................... .................... <br />Analytes reported as N.D. were not present above the stated limit of detection. <br />SEQUOIA <br />Mike GI <br />Project <br />ELAP #1210 <br />41 <br />N. D. <br />0.068 <br />0.21 <br />1.4 <br />CS -C12 <br />Control Limits % % Recovery <br />70 130 92 <br />Page <br />16 <br />