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110 2nd Avenue th,#D7,Pacheco,CA 94553-5560 <br /> 14 1 McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htto://www.mccampbell.wm E-mail:main@mccampbell.com <br /> IT Corporation Client Project ID:#799511-91;PB- Date Sampled: 01/05/01 <br /> 4005 Port Chicago Hwy. Bourbon Date Received: 01/05/01 <br /> . <br /> Concord,CA 94520-1120 Client Contact:Rob Delnagro Date Extracted:01/05/01 <br /> Client P.O: Date Analyzed:01/05/01 <br /> Volatile Organics By GC/MS <br /> ` EPA method 8260 <br /> Lab ID 57335 <br /> Client ID PBG-1 (3 V,) <br /> _ Matrix S <br /> Compound Concentration* RNaa°gL,mm Compound Concentration• RCp010ogt'in°` <br /> W S W S <br /> Acetone 5.0 25 trans-1,3-Dichlompropene 1.0 5.0 <br /> ` Benzene ND 1.0 5.0 Ethylene dibromide 1.0 5.0 <br /> Bminobenzene -- 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> Bromochloromethane --- 1.0 5.0 Hexachlorobutadiene 5.0 25 <br /> Bromodichloromethane ---- 1.0 5.0 lodomethane 1.0 5.0 <br /> Bromaforn ----- 1.0 5.0 Isopropylbenzene 1.0 5.0 <br /> Bromometume --- 1.0 5.0 1 p4sopropyl toluene 1.0 5.0 <br /> n-Butyl benzene 1.0 5.0 Methyl butyl ketone 1.0 5.0 <br /> sec-Butyl benzene 1.0 5.0 Methylene Chloride -- 1.0 5.0 <br /> tert-Butyl benzene - 1.0 5.0 Methyl ethyl ketone - 2.0 10 <br /> Carbon Disulfide --- 1.0 5.0 Methyl isobutyl ketone W 1.0 5.0 <br /> Carbon Tetrachloride -- 1.0 5.0 Methyl tert-Butyl Ether(MTBE) ND 1.0 5.0 <br /> Chlorobenzene 1.0 5.0 Naphthalene -- 5.0 5.0 <br /> Chloroethane 1.0 5.0 n-Propyl benzene -- 1.0 5.0 <br /> 2-Chlomethyl Vinyl Ether"' - 1.0 5.0 Styrene 1.0 5.0 <br /> Chloroform - 1.0 5.0 1,1,1,2-Tetrachloroethane ---- 1.0 5.0 <br /> r, Chloromethane -- 1.0 5.0 1,1,2,2-Tetrachloroethane 1.0 5.0 <br /> 2-Chlorotolume 1.0 5.0 Tetrachloroethene -- 1.0 5.0 <br /> 4-Chlorotoluene l.0 5.0 Toluene ND 1.0 5.0 <br /> Dibronwchloromethane -- 1.0 5.0 1,2,3-Trichlorobmzene - 5.0 25 <br /> 1,2-Dibromo-3chlompropane - 2.0 10 1,2,4-Trichlorobenzene -- 5.0 25 <br /> Dibromomethane 1.0 5.0 1,1,1-Trichloroethane --- 1.0 5.0 <br /> 1,2-Dichlombenzme -- 1.0 5.0 1,1,2-Trichloroethane - 1.0 5.0 <br /> 1,3-Dichlorobenzene 1.0 5.0 Trichloroethene 1.0 5.0 <br /> 1,4-Dichlorobenzene 1.0 5.0 Trichlorofluoromethane 1.0 5.0 <br /> Dichlorodifluoromethane 1.0 5.0 1,2,3-Trichloropropane I.0 5.0 <br /> 1,1-Dichloroethane --- 1.0 5.0 1,2,4-Trimethylbenzene 1.0 5.0 <br /> 1,2-Dichlomethane 1.0 5.0 1,3,5-Trimethylbenzene --- 1.0 5.0 <br /> �- 1,1-Dichloruethme 1.0 5.0 Vinyl Acetate --- 5.0 25 <br /> cis-1,2-Dichlomethme - 1.0 5.0 Vinyl Chloride ° -- 1.0 5.0 <br /> hens-1,2-Dichlomethme 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichlompropme --• 1.0 5.0 Comments: <br /> 1,3-Dichloropropme -- 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane5.0 Dibromofluoromethane 99 <br /> 1,1-Dichloropropene I.0 5.0 Toluene-d8 99 <br /> cis-1,3-Dichloropropene - I.0 1 5.0 1 4-13romofluorobmzene 124 <br /> r <br /> water and vapor samples arc reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipc and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> ` (b)2-prepanone or dimethyl ketone; (c)(2-chloroethoxy)efl me;(d)2-hexanone,(e)dichloromethane; (f)2-butanone; (g)4-methyl-2- <br /> pentanone or isopmpylacetone;(h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than-5 vol. <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethinyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />