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X"LNIL�D VERIFICATION LABORATORY-4-NAL•YS S <br /> I I oe'fr.;lATGl <br /> is ryf?'BE, I ML7AD•t ! PCB <br /> T.�'dX TAVK TPH-C T°H-L I BTX &E I CL HC I TOTAL I M 8E I t3+.DIIsE. it ICA.' 327 <br /> CON'ENTS 8015 80_ 18020 8010 LEAD 907A pTae. AES 19CSC <br /> 3260 82� 9260 19240 7420 8260 9260 l or <br /> A <br /> 860 � 742L 8260 AA <br /> x X <br /> LEADED GAS X I X <br /> UVL� GAS x x <br /> X <br /> i DIESEL X x <br /> x I 1 <br /> K:.gOSENE x Y i <br /> —� <br /> X <br /> UNK FUEL X X x Y <br /> X X PROD. CUL )' <br /> CHLOR. I x <br /> SOLVE I: X X I <br /> NONCHLOR ! x <br /> SOLVENTS X x <br /> WASTE` x X <br /> USED OIL X X X X <br /> All analysis methods are the des!gaat-d EPA methods described!a EPA SW $46.Third Edition. Those methods blot fow'td in <br /> 5)t'9-6 are speefically noted below, Re!= to the "SWRCB LUFT Feld Mdaual'. Appendix D (B), Toole 3-3 on page A''_0 for <br /> mia an m aetsction limlts ter motor vehicle f e! (gasoline and diesel). Refer to "Tri-Regional Board Staff Recommendations for <br /> Init al zvaluation ad IavesdZurcn of L'ST's' for the was a and motor oil tnirimum detection limits. <br /> Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will' be accepted, <br /> howcser laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TE1tMIINZGLOGY: <br /> TPN;-G Total Penclaum Hydrocarbon, UaSoiine. GCFID(5030) 8055 mod or GC!b15 60 <br /> 70F.-E) Total Pa�roleum Hvdmoarbon, Ciesel. GC=!1530). 8015 mod or GC•R�IS 3260 <br /> BTX,4 E Benzene.Toluene,Xylene Sc Ethyl Benzene, C,?ID $020 or GCMS 8=60 <br /> CL HC Chlorinated Hydrocarbon, GC:,,iSD solo, GC'hts$240 or 3260 <br /> TOTAL LEAD Tata; laid.A.4 7420. AA 7421 or ICP-AFS 6010 <br /> OXYGENATES MTBE,ETRE.TA.Ia.DV-,do T3A GC.MS 3250(For MTB+S -r or v you=y use 8020) <br /> METALS ICAP or AA Dtductivply Coupled Plasma.Atomic Emission Spectrometry 6010 or Atomic Abscrprioh Spectromevy 7CC0. <br /> Metals- Cadmium, Chromium III and VI,Load, Zino and vckil. <br /> oCy Poiychiorinaied Biphenyls, WNIS 8270 or 8^83 <br /> GC-FM Gas Cbrcmw.ographv,Flame Ionization Detecdoo <br /> Mstwd 3050 Acid dfgestien <br /> Y.cmod 3340 Soahicc sample preparation <br /> lfemed 3530 Sori_uioh samp'e preparation,extricdon mctho! <br /> tuledred 3030 Purge and trap sampie preparation <br /> Q !QC Quality A531ff1ace.'Ciu1i1ry Camrci <br /> Noes: To avoid false Pus:tive detection of benzene,be,-eme frcc solvrnn are w be used. Fused cariitary coluMns ue?re's-:cd To packed <br /> •Mldmns:a packed co:urrm may be used as a"first cut'with "diary" samples o:ots::tM hydrocarbons have bcen.�ta:acterizeC and proper <br /> Q,{;QC is fo1owed• r-feredoe to the 600 series ceuuse the <br /> For it:nkin:•Rarer sources,EPA raommends Car rhe 300 series for volatile Organic of should be used in p - y rc4'-r <br /> dete::ior limits are lower and the QAAC is beucr. Samples exhibizrg Ery ievei of heavy .rsa; con:=nadon m e`urther arvil�su. <br /> rexmmerxs holding those samples unnt disposal :s indicated. <br /> EH Z3 046 iRevsed OVI3i99: Pxtc s <br />