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GebAnalytical Laboratories;-inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# P112-10 Oxygenates Date: 4/24/03 <br /> Thorpe Oil Project: 541 E. Harding Wy- Stockton Date Rec'd: 4/22/03 <br /> PO Box 357 Date Started: 4/24/03 <br /> Lodi CA 95241 PO# Date Completed:4/24/03 <br /> Date Sampled: 4/22/03 <br /> Sampler: R.Azevedo(Geo) <br /> Sample ID Lab ID RL Method Analyte Results Units <br /> TK 1 ® 8' P200612 10 8260B Methyl tert-butyl ether(MTBE) ND µg/Kg <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(RIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate A=t Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d, 20 19.2 96.0 66-133 <br /> 2-Bromo-1-diloropropane 20 19.4 97.0 63-139 <br /> 4-Bromofluorobemene 20 18.5 92.5 64136 <br /> Stock Pile #1 P200613 10 8260B Methyl tert-butyl ether(MTBE) ND µg/Kg <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl tert-butyl ether(ME) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate A=t Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d, 20 19.8 99.0 66-133 <br /> 2-Bromo-l-chloropropane 20 23.0 115.0 63-139 <br /> 4-Bromofluorobenzene 20 17.5 87.5 64136 <br /> ario D'On� Donna Keller <br /> Chemist Certification # 1157 Laboratory Directors/ <br />