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blIlYAvIU� "ERIFZCATTON LABORATORY ANALYSIS— ri <br /> TAk\fK TANK I *M' ddWE I CL HC im "MTALS <br /> /f CONT.tN. TS - 8t)d l 8015 8020 8010 [CAP/ g270 <br /> 6a' 8260 8260 8240 ^420 ES or 8080 <br /> 78,1 AA <br /> I <br /> LEADED GAS X I X I X X <br /> t NL GA5 X <br /> DIESEL X I C <br /> KEROSENrz X X <br /> FUEL x ,.,. k. <br /> PROD. CM X X � <br /> CHLOR. <br /> SOLVENTS X I X <br /> NONCHLOR <br /> SOL'�ENTS X <br /> X <br /> � I X <br /> WAII I r <br /> USED OIL X K X x x X X <br /> All analysis methods are the desigsrarat EPA t ededs described in EPA SW 84c, Third Edition. Those mecbads sac fntmd itf <br /> SW $46 me specifically acted below. Refer to the -SWRCS LUFT Feld MaaunL•, Appendix D (B), Table 1-5 ca page AZO for <br /> minimum deseccm limits for motor vehicle &sl(psolitte and diesel). Refer m 1-2-3 'Regional Board Stan Recvmuendarioes <br /> for I6i[iaL Evaltradda and Iavestfgauon of UST's' for the waste and tactor oil Mimmam de=don limits. <br /> Detecdon Limits that remain belaw the MCL. STLC or Allowable Limit of ttte corrtamiaaat in question will be accepted, <br /> how"4=laboratory sban uttilze the mint caoserragTe method. <br /> LABORATORY ANALYSES TE}UMCLOGY: <br /> TPH-C TOW Pendkwa Hydmcrton, Gawiioa GC1FID(1030) 8011 mod or GC,'MS r60 <br /> t7H'O Total Purtroleurn Hydro carbon_ blew!,GC/FID(3350), 8015 mod or GUMS 8260 <br /> BTX at E .. Bestzene,Toldeoe.Xylem do Ethyl Bsmsee, GC-?M 8020 or GCIMS 8260 <br /> CL HC gttorimred Hydrocarbon-GCIHSD $010. GCM8 3240 <br /> TOTAL LEAD Total lead. ,kA 7420, AA 7421 or ICP-AFS 6010 ' <br /> M7ME,TAME,DIPE,THA GAMS 8260 . <br /> METALS ICA?or AA Inductively Coupled Plasma Aremic Emission Spaaomeay 6010 or Atomic Absorption Spectrometry 7000. <br /> ?r-3 ,IVEMW C2dmfam, Chromium III and YU Lead, Zinc and Nickel. <br /> Polychlorinated Biphenyls,GCN3 8270 or$080 <br /> GG FID Gas Chromatography, flame bsnization Detection <br /> Method 3030 Arad digtvdon <br /> Method 3540 Soxhler tarnpk preparation <br /> ?Method 3550 50711ca600 Sample Pm-Panum. extraction method <br /> Method 5030 Purge and trap sample preparmon <br /> QA/QC Quality AmuntacrlQuit iry Conaoi <br /> Norex; TO avoid false positive ciecct:on of bern;erre, benzene•free solvents are to be uxd. Fwednpj <br /> OAJQC 4 folloed. ilary mlunvm are preferred to Peeked <br /> coltunrs: a packed column may he used a I f!mt ease" Wi%b 'dirty, e ole hydr <br /> ,Anitites or oraoc:.rCons haw been charu:erizcd and proper <br /> w <br /> For drinkfnir wyrsr saurrts. EPA recommends chat the 500 seep for volAnle argmic theuld be used in preference to the 500 series because rhe <br /> detecidn limos am lower and the QA/QC is better. Samples wfbi(ingany leve{di heavy metal contamitumn may require further aaaivsts. <br /> F1'S-MM reeammends holding those samples umil disposal is indicated. <br /> EH 77 OL6 (Revised SOH Sygg) Page 8 <br />