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_ wrocrznnt 0y:46 5720916 GEOANALVTICAL LAB <br /> PAGE 03 <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209(572-0900 Fax(209)572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report• M19&13 Oxygenates Date: 4/25/01 <br /> Date Rev'd. 4/19/01 <br /> Thorpe Oil Project Old Chase Chevy Bldg.,Stockton Date Started 4/24/01 <br /> PO Box 357 Date Completed: 4/25/01 <br /> Lodi CA 95241 pO# <br /> Date Sampled: 4/18/01 <br /> Time: <br /> Sampler : R Chrun(Gw) <br /> Sample ID: TK south at 101/2' <br /> Lab ID. M201462 <br /> Method RL Analyte Results Units <br /> 8260E 10 Methyl tent-butyl ether(MTBE) ND P8/Kg <br /> 100 Ethanol ND <br /> 100 tent-Butanol ND <br /> 10 di-Isopropyl ether(DIPS) ND <br /> 10 Ethyl tat-butyl ether(ETBE) ND <br /> 10 tent Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery Limit <br /> 1,2dAddoroethane-d4 100 111 ill 66-133 <br /> 2-Bromo-l-chWmpmpane 100 101 101 63-139 <br /> ///i/ �^�^ A-Hronwfluoeobenr�e 100 105 IDS <br /> 64-136 <br /> Mario D'OnoffriL Donna Keller 1 <br /> Chemist Certification 4 1157 Laboratory Director <br />