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05/02/2001 09:46 5720916 GEGANALVTICAL LAB PAGE 04 <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Fax(2091572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report; Mloo-13 Oxygenates DgC 4/25/01 <br /> Date Recd: 4/18/01 <br /> Thorpe Oil Pmject Old Chase Chevy B1dg.,Stockton Date Started:- 4/2,101 <br /> Date Completed: 4/25/01 <br /> PO Bax 357 <br /> Lodi CA 95241 PO# <br /> Date Sampled: 4/18/01 <br /> Time: <br /> Sampler : R Chrun(Geo) <br /> Sample ID: SP <br /> Lab ID: M201463 <br /> Method RL Analyte Results Units <br /> ■ <br /> 8260E 10 Methyl tert-butyl ether(MTBE) ND 1t8/KS <br /> 100 Ethanol ND <br /> 100 tert-Butanol ND <br /> 10 di-lsopropyl ether(D1PE) ND <br /> 10 Ethyl tent-butyl ether IETBE) ND <br /> 10 tert-Amyl mathyl ether(TAME) NP <br /> Surrogate Amnt Spiked AmntRecovered 96 Recovery Limit <br /> 1,2-Dichloroethane-d, 100 111 111 66-133 <br /> 2-11romo-l-chloropmpane 100 107 107 63-139 <br /> 4-Bromolluamheatzene 100 103 103 64.136 <br /> oris D'Qito Donna Keller <br /> Chemist Certification A 1157 Laboratory Director <br />