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110 2nd Avenue So #D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htto://www.MEggMpbell.com E-mail:mainQmccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:RMB Date Sampled:04/12/01 <br /> 837 Shaw Road Date Received: 04/12/01 <br /> Stockton, CA 95215 Client Contact:Bob Marry Date Extracted:04/12/01 <br /> V <br /> Client P.O: Date Analyzed: 04/13-04/17/01 <br /> r <br /> Diesel Range(C10-C23)and Oil-Range(C18+)Extractable Hydrocarbons as Diesel and Motor Oil* <br /> EPA methods modified 8015,and 3550 or 3510;California RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d) TPH(mo)+ %Recovery <br /> Surrogate <br /> 65329 Tl-W S 550,gd 1800 83 <br /> 65334 WOl S 4.6,c/e 7.6 103 <br /> 65335 SP1-W S 94,g 390 119 <br /> L 65336 SP1-E S 7.3,g 56 I00 <br /> L <br /> r <br /> r. <br /> Reporting Limit unless otherwise W 50 ug/L 250 ug/L <br /> stared;ND means not detected above <br /> the reporting limit S 1.0 mg/kg 5.0 mg/kg <br /> *water samples are reported in ug/L,wipe samples in ug/wipe,sail and sludge samples in mg/kg,and all TCLP/STLC/SPLP extracts in <br /> ug/L <br /> "cluttered chromatogram resulting in coeluted surrogate and sample peaks,or.;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> `The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant b)diesel range compounds are significant;no recognizable pattern;c) <br /> aged diesel?is significant);d)gasoline range compounds am significant;e)medium boiling point pattern that does not match diesel(fuel <br /> oil?);f)one to a few isolated peaks present g)oil range compounds aro significant;h)lighter than water immiscible sheen is present; i) <br /> liquid sample that contains greater than—5 vol.%sediment. - <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />