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110 2nd Avenue So #D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> bttp://www.m22gMpbell.corn E-mail:mainQamccampbell.com <br /> Advanced GeoEnvirolmtental Client Project ID:RMB. <br /> Date Sampled:04/12/01 <br /> 837 Shaw Road Date Received:04/12/01 <br /> Stockton,CA 95215 Client Contact:Bob Marty Date Extracted:04/12/01 <br /> loss <br /> Client P.O: Date Analyzed: 04/13-04/16/01 <br /> Volatile Organics By GC/MS <br /> `. EPA method 8260 <br /> Lab ID 65331 <br /> Client ID <br /> Matrix ` <br /> Compound Concentration* Repning Limit Compound Concentration* Reporting Limit <br /> W S w 5 <br /> Acetone a1 ND<38,000 5.0 25 trans-1,3-Dichlompropene ND<5000 1.0 5.0 <br /> Benzene ND<5000 1.0 5.0 Ethylene dibrotnide ND<5000 1.0 5.0 <br /> Bromolxnzene ND<5000 1.0 5.0 Ethylbenzene 200,000 1.0 5.0 <br /> Bromachloromedume ND<5000 1.0 5.0 Hexachlorobutadiene ND<5000 5.0 25 <br /> Bromodichlorornethane ND<5000 1.0 5.0 lodomethane ND<5000 1.0 5.0 <br /> �.. Bromoform ND<5000 1.0 5.0 lsopropylbenzene NIK5000 1.0 5.0 <br /> Bromomethane ND<5000 1.0 5.0 p-Isopropyl toluene 23,000 1 1.0 0 5.0 <br /> n-Butyl benzene 25,000 1.0 5.0 Methyl butyl ketone ND<5000 1.0 5.0 _ <br /> sec-Butyl benzene N13<5000 1.0 5.0 Methylene Chloride` ND<8400 1.0 5.0 <br /> tert-Butyl benzene ND<5000 1.0 5.0 Methyl ethyl ketone ND<5000 2.0 10 <br /> Carbon Disulfide ND<5000 LO 5.0 Methyl isobutyl ketone ND<5000 1.0 5.0 <br /> Carbon Tetrachloride ND<5000 1.0 5.0 Methyl tert-Butyl Ether(MTBE) -- I.0 5.0 <br /> Chlorobenzene N13<5000 1.0 5.0 Naphthalene 27,000d5.O <br /> 5.0 <br /> Chloroethane ND<5000 1.0 5.0 n-Propyl benzene 70,0005.0 <br /> 2Lhloroethyl Vinyl Eth ND<5000 t.0 5.0 Styrene ND<5000 5.0 <br /> Chloroform ND<5000 1.0 5.0 1,1,1,2-Tehachloroethane ND<5000 5.0 <br /> Chloromethane NDc5000 1.0 5.0 1,1,2,2-Tetrachloroethane ND<5000 5.0 <br /> 2-Chlorotaluene NIK5000 1.0 5.0 Tetrechloroethene NW 000 5.0 <br /> 4-Chlormoluene ND<5000 1.0 5.0 Toluene 99,000 5.0 <br /> Dibmntochloromethane ND<5000 I.0 5.0 1,2,3-Trichloroberunme ND<5000 25 <br /> 1,2-Dibromo-3-chloropropane ND<5000 2.0 10 1,2,4-Trichlombenzene ND<5000 25 <br /> Dibromomethane ND<5000 ]A 5.0 1,1,1-Trichloroethane ND<5000 1.0 5.0 <br /> 1,2-Dichlorobenzene ND<5000 1.0 5.0 1,1,2-Trichloroethane ND<5000 1.0 5.0 <br /> 1,3-Dichlorobenzene ND<5000 1.0 5.0 Tnchlomethene ND<5000 1.0 5.0 <br /> 1,4-Dichlorobenzene ND<5000 1.0 5.0 Trichlorofluoromethane ND<5000 1.0 5.0 <br /> 1100 Dichlorodifluoromethane ND<5000 1.0 5.0 1,2,3-TrichloropmWe ND<5000 LO 5.0 <br /> 1,1-Dichlomethane ND<5000 1.0 5.0 1,2,4-Trimethylberuene 330,000 1.0 5.0 <br /> 12-Dichlomethme ND<5000 1.0 5.0 1,3,5-Trimethylbenzene 130,000 1.0 5.0 <br /> 1,1-lhchlomethene ND<5000 1.0 5.0 Vinyl Acetate m ND<5000 5.0 25 <br /> cis-1,2-1Nchloroethene ND<5000 1.0 5.0 Vinyl Chloride ° ND<5000 1.0 5.0 <br /> -tram ND<5000 1.0 5.0 Xylenes,total 1,100,000 I.0 5.0 <br /> 12-Dichloropropane ND<5000 1.0 5.0 Comments: <br /> ` 1,3-Dichloropropane ND<5000 1.0 5.0 Surrogate Recoveries(%) <br /> 22-Dichlompropme ND<5000 1.0 5.0 Dibrorrafluoromethane 99 <br /> 1,1-Dichlompropme ND<5000 1.0 5.0 Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND<5000 1.0 1 5.0 4-Bromofluorobenzene 107 <br /> Iss, water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug(L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propmone or dimethyl ketone; (c) (2chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butane; (g) 4-methyl-2- <br /> penumone or isopmpylacctone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than-5 vol.% <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; 0) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chlomethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> r <br />