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SAN JOAQUIN LOC.AZ. HM•TH DISTRICTI' <br />MININUi VERIFICATION LABORATORY ANALYSIS <br />TANK CONTENTS <br />Waste Product <br />TPH-G <br />OC -FID <br />(5030) <br />TPH-D <br />OC -FID <br />(50 30) <br />TEPH <br />(3550) <br />(3540) <br />BTUE <br />(8020) <br />CL HC <br />(8010) <br />(8240) <br />TEL <br />(D <br />EDB <br />H S) <br />METALS <br />(ICP- <br />AM I <br />PCB <br />(8270) <br />LUM GASOLINE <br />X <br />Total Petroleum Hydrocarbon, Diesel <br />Im <br />X <br />M 6 6 (8020) <br />X <br />X <br />Chlorinated Hydrocarbon 8010 or 8240 <br />TYL (DOHS-LUFT) <br />UL GASOLINE <br />X <br />Ethylene dibromide (DOHS -AH 1803) <br />QC FID <br />X <br />ICP—A68 OR AA <br />Inductively Coupled Plasma Atomic Emission Spectrometry or Atomic <br />Absorption Spectrometry <br />Method 5030 <br />DIJQeQ. <br />Method 3550 <br />Sonication Sample Preparation <br />X <br />X <br />QA/X <br />Quality Assurance/Quality Control <br />!(IROMM <br />X <br />X <br />UA(HORN FUEL <br />X <br />x <br />X <br />X <br />x <br />OIL <br />X <br />X <br />CHLOR. SOLVENTS <br />X <br />X <br />11ONCK.OR. SOLVTS <br />--*-- <br />---- <br />----- <br />-- <br />WASTE/USED OIL <br />X <br />X <br />X <br />X <br />X <br />MINIMUM VERIFICATION LABORATORY ANALYSES TERMINOGO(;Y <br />The following listing of <br />laboratory analyses abbreviations Is provided as a guide so that <br />terminology used will be <br />more familiar. All analyses methods are designated EPA methods as <br />described in EPA SW 846, <br />Third Edition. Those methods not found In SM 846, are <br />specifically noted. <br />TPH G <br />Total Petroleum Hydrocarbon, Gasoline <br />I" D <br />Total Petroleum Hydrocarbon, Diesel <br />Im <br />Total Extractable Petroleum Hydrocarbon (8015) <br />M 6 6 (8020) <br />Benzene, Toluene, Xylene a Ethyl Benzene (8020) <br />CL HC 8010 OR 8240 <br />Chlorinated Hydrocarbon 8010 or 8240 <br />TYL (DOHS-LUFT) <br />Tetraethyl Lead (DOHS-LUFP) <br />=8 (DOHS -AB 1803) <br />Ethylene dibromide (DOHS -AH 1803) <br />QC FID <br />Gas Chromatography, Flame Ionization Detector <br />ICP—A68 OR AA <br />Inductively Coupled Plasma Atomic Emission Spectrometry or Atomic <br />Absorption Spectrometry <br />Method 5030 <br />Purge and Trap Sample Preparation <br />Method 3550 <br />Sonication Sample Preparation <br />Method 3540 <br />Soxhlet Sample Preparation <br />QA/X <br />Quality Assurance/Quality Control <br />Motes: To avoid false positive detection of benzene, benzene -free solvents are to be used. <br />Fused capillary columns are preferred to packed columns; a packed column may be used as a <br />•first cut" with "dirty* samples or once the hydrocarbons have bean characterized and <br />Proper QA/QC Is followed. <br />For Drinking Mater Sources, BPA recommends that the 500 series for volatile <br />Or"nlcs be used in preference to the 600 series because the detection limits are lover and <br />00 04/0C is better. <br />SITE ADDRESS 541 N. Hutchins, Lodi, CA <br />Sweeps q___ <br />#1 23 048 12/88 Contractor: JIM THORPE OIL, INC. Approval date <br />