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2. Boll - <br /> bse .EPIC method 3550, sonication ztractf= <br /> manusi 8W-84d, April 1984) : - Aoatone (FPA <br /> �►fth sample pnztitfon axtractim- <br /> to be a$ a=aptabls in hem. found <br /> other appropriate solven�lma �.paratioa, h ver <br /> _- Y also ha veld. <br /> B. <br /> Per also d <br /> 3c operations -for etection o= t <br /> ittel hydr1 <br /> tactor= Flax* Ionisation <br /> Column: '10 Percant sP2100 an 80.100 apt r Via« <br /> glass sup&lcoport. <br /> ueed as a substitute &illary columns say also b,& <br /> e se <br /> Carrier Gas: Nitrogen at 3to inprovPotion. <br /> r Temperature:- 250 C <br /> DOUCtor T6MP rat=-eu 30 C <br /> _1QQCM � <br /> Tratura: 40 C hold for 3 miriu <br /> _4ap rata to 300% or =til at Iaagt 958 <br /> of all comporAnta are alatad. <br /> inQuantify Total . Petroleum pus, Hydrocarbrh <br /> eq� � all detectable b <br /> Period which Ott leant 95of viten the <br /> time _ <br /> IIaasd ns are eluted. Cslibrattioi�recovarable <br /> upon an aPF�priate �� 'shall - be <br /> representative of -the suspect fuel. 'tandard <br /> If apt aPpz'opr3at& sail• for calibration does . <br /> nvt exist, as in thr Casa- of as <br /> calibration shall bs don• us a9ed . . 3. <br /> representative fne.l standard. a A°`n`agedw <br /> Calibration should be established sithin the <br /> estimated rang& of contaminant <br /> sesPle, based on odor or- Z is �rithift the <br /> _ measeremants or on Prascre <br /> method) , (i.e. Or <br /> combustab" � sitar. or I.R <br /> are Pharr nen-dStectable aoneentrat own <br /> exceed ��, 'the level of 'detection shall <br /> for soil and 30 ppb for vatsr. <br />