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M19UM VERIFICATION LABORATORY A is <br /> EDB METALS PCB <br /> TPH-G TPH-D BTX & E CL HC TOTAL ICRP/ 8270 <br /> TANK TANK 8015 8015 W20 8010 LEAD <br /> 7420 8240 AES or 8080 <br /> # CONTENTS 8260 8260 8260 8240 . 7421 <br /> LEADED X X X <br /> GAS X <br /> UNL GAS <br /> X X <br /> 559 DIESEL <br /> X X <br /> X <br /> KEROSENE X X X <br /> UNK FUEL <br /> X X X <br /> PROD. OIL <br /> X X <br /> CHLOR. X X <br /> SOLVENTS <br /> NONCHLOR X X X <br /> SOLVENTS <br /> WASTE\ X X <br /> USED OIL <br /> X X X X <br /> All analyses methods are designated EPA methods described in EPA SW 846,Third Edition. Those methods -5 Lound <br /> in SW 846, are specifically no below. Refer to the "SWRCB LUFP Field Manual", Appendix A-20,Table 3-$ for <br /> fer to 1-2.3 <br /> detection <br /> wali anon motor vehicle fuels <br /> of(USTsine a <br /> for the waste and nd diesel). emotor oil detection limits.ional Staff <br /> Rwill be accepted, <br /> Initial E <br /> 1)etection Limits that remain however laboratory shalltllizbelow <br /> e lthe mosticonservative method ble limit o[the contaminant to question <br /> LABORATORY ANALYSES TERMINOLOGY: 5030 8015 mod or GC/MS060 <br /> Total Petroleum Hydrocarbon, <br /> TPH-G Gasoline, GC/FID 550 , 8015 mod or GGM S <br /> TTH-D Total Petroleum Hydrocarbon, Diesel, GC/FID ( ) S 8260 <br /> BTX & E Benzene,Toluene, Xylene & Ethyl Be one,, S ID4 or GCJM <br /> CL HC Chlorinated Hydrocarbon, GC/H <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES01140 DHS-LUFT) <br /> EDB Ethylene dibromide (DHS-AB 1803), GC/MS <br /> GC-FID Gas Chromatography, Flame Ionization Detection <br /> ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Chromium III and VI, Lend, Zinc and Nickel. <br /> Spectrometry 7000. Metals: Cadmium <br /> PCB <br /> Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of benzene, benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns, a packed column may be used as a "first cut" with "duty" samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the <br /> 600 <br /> detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br /> series because the D recommends holding these samples until disposal is indicated. <br /> contamination may require further analysis. PHS-EH <br /> EH 23 048 (Revised 7/10/92) Page 8 <br />