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' 110 2nd Avenu i1D7,Pacheoo,CA 44553-5560 <br /> 798 <br /> McCampbell Analytics c. -1622 <br /> Telephone:4 3-com E-mail:Fax:9(a ftwcampb <br /> h :Ilwww,mcca bell.com E- main campbell.com <br /> Shaw Environmental Client Project ID: #844915; SBC-Stockton Date Sampled: 07/31/03 <br /> 4005 Port Chicago Hwy Date Received: 07/31/03 <br /> Client Contact: Rob Delnagro Date Extracted: 07/31/03 <br /> Concord, CA 94520 <br /> Client P.O.: Date Analyzed: 07/31/03 <br /> Gasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline with BTEX and MTBE* <br /> Extraction method: SW5030B Analytical methods: SW8021B/8015Cm Work Order. 0307538 <br /> Lab ID Client ID Matrix TPH(g) MTBE Benzene Toluene Ethylbenzene Xylenes 1w %SS <br /> OOIA TP-1(14') S ND ND ND ND ND ISD 1 10.0 <br /> 002A TP-2(t4') S ND ND ND ND ND ND 1 12.2 <br /> 003A DI-t(3 112') S ND ND ND ND ND ND 1 77.5 <br /> Reporting Limit For DF=1; W NA NA NA NA NA NA 1 ug/L <br /> ND means not detected at or <br /> above the reporting limit S 1.0 0.05 0.005 0.005 0.005 0.005 1 mg/Kg <br /> water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples inµg/kg, wipe samples in ltg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> #cluttered chromatogram;sample peak coelutes with surrogate peak. <br /> +The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation:a) <br /> unmodified or weakly modified gasoline is significant;b)heavier gasoline range compounds are significant(aged gasoline?);c)lighter gasoline range <br /> ' compounds(the most mobile fraction)are significant;d)gasoline range compounds having broad chromatographic peaks are significant;biologically <br /> altered gasoline?;e)TPH pattern that does not appear to be derived from gasoline(stoddard solvent/mineral spirit?);f)one to a few isolated non-target <br /> peaks present;g)strongly aged gasoline or diesel range compounds are significant;h)lighter than water immiscible sheen/product is present;i)liquid <br /> sample that contains greater than—2 vol.%u sediment;j)reporting limit raised due to high MTBE content;k)TPH pattern that does not appear to be <br /> derived from gasoline(aviation gas).m)no recognizable pattern. <br /> DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />