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110 2nd Aven #D7,Pacheco,CA 94553-5560 <br /> rA# McCampbell A nalytica C. Telephone.9 - 98-1620 Fax:925-798-1622 <br /> http://www.mccauVbeU.com E-mail:ma!2.emccampb4l.corn <br /> Shaw Environmental Client Project ID: #844915;SBC-Stockton Date Sampled: 07/31/03 <br /> 4005 Port Chicago Hwy Date Received: 07/31/03 <br /> Client Contact: Rob Delnagro Date Extracted: 07/31/03 <br /> Concord,CA 94520 <br /> Client P.O.: Date Analyzed: 07/31/03 <br /> Gasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline with BTEX and MTBE* <br /> Extraction method: SW5030B Analytical methods: SW8021B/8015Cm Work Order: 0307539 <br /> Lab ID Client LD Matrix TPH(g) MTBE Benzene Toluene Ethylbenzene Xylenes DF %SS <br /> 001A CS(l-4) S ND ND ND ND ND ND 1 93.1 <br /> 002A CS(5-8) S ND ND ND ND ND ND 1 96.0 <br /> Reporting Limit for DF=1; W NA NA NA NA NA NA I ug(L <br /> ND means not detected at or <br /> above the reporting limit S 1.0 0.05 0.005 0.005 0.005 0.005 1 mg/Kg <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in pg/kg, wipe samples in pg/wipe, <br /> prod uct/oillnon-aqueous liquid samples in mg/L. <br /> #cluttered chromatogram;sample peak coelutes with surrogate peak. <br /> +Tire following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation:a) <br /> unmodified or weakly modified gasoline is significant;b)heavier gasoline range compounds are signifcant(aged gasoline?);c)lighter gasoline range <br /> compounds(the most mobile fraction)are significant;d)gasoline range compounds having broad chromatographic peaks are significant;biologically <br /> altered gasoline?;e)TPH pattern that does not appear to be derived from gasoline(stoddard solvent/mineral spirit?);f)one to a few isolated non-target <br /> peaks present;g)strongly aged gasoline or diesel range compounds are significant;h)lighter than water immiscible sheen/product is present;i)liquid <br /> sample that contains greater than--2 vol.%sediment;j)reporting limit raised due to high MTBE content; )TPH pattern that does not appear to be <br /> derived from gasoline(aviation as).m)no recd pattern.atte . <br /> DHS Certification No. 1644 Angela Rydelius, Lab Manager <br />