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Alpha Analytical, Inc. 10 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 (775) 355-1044 • (775) 355-0406 FAX• 1-800-283-1183 Dale: 20-Nov-0/ QC Summary Report Work Order: 01110963 Method Blank - Type:MBLK Test Code:SW0260B Batch ID:MS9S7109A File ID:D:kHPCHEMIMS09kDATA1011109101110935.D Analysis Date: 111091200122:40 Sample ID: MBLK MS9S1109A Units:pg/Kg Run ID:GC/MSD_9_011109B Prep Date: 11/09/2001 Anatyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Tertiary Butyl Alcohol(TBA) ND 500 Methyl tert-butyl ether(MTBE) ND 5 Di-isopropyl Ether(DIPE) ND 20 Ethyl Tertiary Butyl Ether(ETBE) ND 20 Benzene ND 5 Tertiary Amyl Methyl Ether(TAME) ND 20 Toluene ND 5 Ethylbenzene ND 5 m,p-Xylene ND 5 o-Xylene ND 5 Laboratory Control Spike Type:LCS Test Code:SW8260B Batch ID:MS9S1109A File ID:D:kHPCHEMIMS091DATAk011109101110936.D Analysis Date: 11/09/200123:02 Sample ID: LCS MS9S1109A Units:pg/Kg Run ID:GC/MSD_9_011109B Prep Date: 11/09/2001 Analyte Result PQL SpkVal SpkReNal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Benzene 189 5 200 95 32 148 Toluene 181 5 200 90 39 136 Ethylbenzene 186 5 200 93 45 152 m,p-Xylene 381 5 400 95 42 154 o-Xylene 193 5 200 97 41 154 Sample Matrix Spike Type: MS Test Code:SW0260B Batch ID:MS9S1109A File ID:D:kHPCHEMkMS0SMATA1011109k01110939.D Analysis Date: 11/10/200100:08 Sample ID: 01110632-06AMS Units:pg/Kg Run ID:GC/MSD_9_01110913 Prep Date: 11/07/2001 Analyte Result PQL SpkVal SpkReNal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Benzene 181 5 200 0 91 32 148 Toluene 174 5 200 0 87 39 136 Ethylbenzene 180 5 200 0 90 45 152 m,p-Xylene 372 5 400 0 93 42 154 o-Xylene 188 5 200 0 94 41 154 Sample Matrix Spike Duplicate Type:MSD Test Code:SW0260B Batch ID:MS9S7109A File ID:D:kHPCHEMIMS09kDATA1011109k01110940.D Analysis Date: 11/10/200100:30 Sample ID: 01110632-06AMSD Units:pg/Kg Run ID:GC/MSD_9_011109B Prep Date: 11/07/2001 Analyte Result PQL SpkVal SpkReNal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Benzene 172 5 200 0 86 32 148 181.4 5.15 Toluene 166 5 200 0 83 39 136 173.9 4.57 Ethylbenzene 171 5 200 0 85 45 152 180.2 5.23 m,p-Xylene 350 5 400 0 87 42 154 372.2 6.25 o-Xylene 176 5 200 0 88 41 154 188 6.56 Comments: ND-Not Detected at the Reporting Limit. D-If the spiced value is<25%ofthe reference value,recovery should not be calculated. S-Spike Recovery outside accepted recovery limits, M-Spike Recovery outside accepted recovery limits due to matrix. B-Analyte detected in the associated Method Blank.