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Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 2t -Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> date: OC ummary RWork Order: <br /> Seport <br /> 16-Dec-07 •7 07121107 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: 07121208.1) Batch ID:MS08S8908A Analysis Date: 12/1212007 10:25 <br /> Sample 10: MBLK.MS08S8908A Units: yg1Kg Run ID:MSD_08_071212B Prep Date: 1211212007 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 500 <br /> Methyl tert-butyl ether(MTBE) ND 5 <br /> Di-isopropyl Ether(DIPS) ND 20 <br /> Ethyl Tertiary Butyt Ether(ETRE) ND 20 <br /> 1,2-❑ichloroethane ND 20 <br /> Benzene ND 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 20 <br /> Toluene ND 5 <br /> 1,2-Dibromoethane(EDS) ND 40 <br /> Ethylbenzene ND 6 <br /> m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Surr: 1,2-Dichloroethane-d4 189 200 95 69 126 <br /> Burr:Toluene-d8 222 200 111 80 120 <br /> Surr:4-Bromofluorobenzene 191 200 95 80 120 <br /> Laboratory Control Spike Type LCS Test Code:EPA Method SW8260B <br /> File ID:07121209.1) Batch ID:MS08SS908A Analysis Date: 12/1212007 10:46 <br /> Sample ID: LCS MS08S8908A Units:pg1Kg Run ID:MSD_08_071212B Prep Date: 12112!2007 <br /> Analyte Result PQL SpkVal SpkRefVat %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Methyi tert-butyl ether(MTBE) 435 10 400 109 63 136 <br /> Benzene 458 10 400 114 70 140 <br /> Toluene 475 10 400 119 70 130 <br /> Ethylbenzene 443 10 400 111 70 130 <br /> m,p-Xylene 468 10 400 117 70 133 <br /> o-Xylene 468 10 400 117 70 135 <br /> Burr: 1,2-Dichioroethane-d4 380 400 95 69 126 <br /> Burr:Toluene-d8 422 400 105 80 120 <br /> Surr:4-Bromofluorobenzene 392 400 98 80 120 <br /> Sample Matrix Spike Type MS Test Cade: EPA Method SW8260B <br /> File ID:07121210.1) Batch ID:MSOBS8908A Analysis Date: 12/12/2007 11:07 <br /> Sample ID: 07120725-07AMS Units: pg1Kg Run ID:MSD_08_071212B Prep Date: 12112/2007 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPR(Limit) Qua! { <br /> Methyl tart-butyl ether(MTBE) 419 10 400 0 105 42 146 } <br /> Benzene 455 10 400 0 114 57 140 <br /> Toluene 476 10 400 0 119 60 130 <br /> Ethylbenzene 443 10 400 0 111 63 134 <br /> m,p-Xylene 468 10 400 0 117 64 136 <br /> o-Xylene 466 10 400 0 116 62 138 <br /> Burr: 1,2-Dichloroethane-d4 381 400 95 69 126 <br /> Burr:Toluene-d8 427 400 107 80 120 <br /> Burr 4-Bromofluorobanzene 389 400 97 80 120 <br /> Sample Matrix Spike Duplicate Type MSD Test Code:EPA Method SW8260B <br /> Fife ID:07121211,1) Batch ID:MS0858906A Analysis Date: 12/12/2007 11:28 <br /> Sample ID: 07120725-07AMSD Units:pg/Kg Run ID:MSD_08 0712129 Prep Date: 12/12/2007 <br /> Analyte Result PQL SpkVal SpkRofVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qua[ <br /> Methyl tert-butyl ether(MTBE) 390 10 400 0 97 42 146 419.4 7.3(20) <br /> Benzene 430 10 400 0 106 57 140 454.9 5.5(20) <br /> Toluene 450 10 400 0 112 60 130 475.8 5.6(20) <br /> Ethylbenzene 411 10 400 0 103 63 134 443 7.5(20) <br /> m,p-Xylene 438 10 400 0 110 64 136 467.7 6.5(20) <br /> o-Xylene 430 10 400 0 107 62 138 465.8 8.0(20) <br /> Burr: 1,2-Dichloroothane-d4 370 400 92 69 126 <br /> Surr:Toluene-d8 428 400 107 80 120 <br /> Burr:4-Bromofluorobenzene 406 400 101 80 120 <br />