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LEVINE-FRICKE <br />slurry was injected into this area to provide structural <br />integrity between the compacted backfill material and overlying <br />loading dock. The piping trench backfill was compacted using <br />Whacker equipment. <br />3.0 CHEMICAL ANALYSES AND RESULTS <br />Soil samples were analyzed for total petroleum hydrocarbons <br />(TPH), using EPA Method 8015 to detect diesel and gasoline, and <br />for purgeable aromatics (benzene, toluene, xylenes and <br />a- ethylbenzene [BTXE]) using EPA Method 8020. Samples were also <br />analyzed for ethylene dibromide (EDB) using EPA Method 8240, and <br />organic lead, using DHS methodology, as requested by the SJLHD, <br />since the tank at one time had apparently stored leaded gasoline <br />(as noted on the former dispenser). Chemical analysis results <br />are summarized in the table on Figure 2, and copies of laboratory <br />certificates are included in Appendix B. <br />Analysis results indicate that TPH as diesel and gasoline were <br />not detected above laboratory detection limits (10 ppm) in any of <br />�. the soil samples, with the exception of sample DI -2.51, collected <br />beneath the former dispenser. Gasoline was reported at a <br />concentration of 390 ppm, and diesel at a concentration of 37 ppm <br />in this sample. <br />Benzene, toluene, xylenes and ethylbenzene were not detected <br />above laboratory detection limits (0.025 ppm for benzene and <br />toluene, and 0.075 ppm for xylene and ethylbenzene) in any of the <br />soil samples, with the exception of 0.065 ppm of toluene reported <br />in sample PP4-31. This concentration of toluene is considered to <br />be low in relation to the RWQCB guidelines for allowable toluene <br />concentrations in soils (0.3 ppm with high leaching potential <br />conditions, as referenced in the December 1987 Leaking <br />Underground Fuel Tank Field Manual). <br />Organic lead was not detected in any of the analyzed soil <br />samples. EDB was detected in three samples (TS -141, PPl-3' and <br />PP4-31) at concentrations ranging from 0.180 to 0.370 ppm, and <br />was not detected above a detection limit of 0.125 ppm in the <br />other samples. <br />3.1 Discussion of Results <br />The presence of 390 ppm of gasoline detected in the soil sample <br />collected from below the dispenser island indicated that limited <br />fuel leakage has occurred in this area. Field observations <br />suggest that this leakage has occurred over a very small area, <br />however, and does not appear to represent a significant release. <br />-4- <br />