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Ivll•IUM VERIFICATION LABOR.ATORYSALYSIS <br />TANK <br /># <br />TANK <br />CONTENTS <br />TPFI-G <br />8015 <br />8260 <br />TPH-D <br />8015 <br />8260 <br />BTX & E <br />8020 <br />8260 <br />CL HC <br />8010 <br />8240 <br />TOTAL <br />LEAD <br />7420 <br />7421 <br />EDB <br />8240 <br />METALS <br />ICRP/ <br />AES or <br />AA <br />PCB <br />8270 <br />8080 <br />'Total lead, AA 7420, AA 7421 or ICP -AES 6010 <br />LEADED <br />GAS <br />X i <br />Gt Tin <br />X <br />ICAP or AA <br />X <br />X <br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel. <br />_- <br />_-^ <br />---- <br />UrA, GAS -- <br />`C <br />Soshlct Sample preparation <br />X <br />` <br />Method 5010 <br />Purge and trap sample preparation <br />Q,t'Qt' <br />- <br />-- - -- <br />DIESEL---- <br />-- <br />X <br />X <br />KF-.ROSFNF <br />X <br />X <br />UNK FUFL <br />X <br />X <br />X <br />X <br />----- <br />OIL <br />-- <br />X <br />X <br />--- -- <br />CALOR. <br />SOLVENTS <br />X <br />X <br />_ <br />-- <br />NONCIILOR <br />SOLVFN'iS <br />X <br />WASTE\ <br />SED 0[I. <br />X <br />X <br />X <br />X <br />X <br />All analyse methods are designated EPA methods described In EPA SW 846, Third Edition. Those methods not found in <br />!;W 81(, are specifically noted helow. Refer to the "SWRCB LUFT Field Manual% Appendix A-20, Table 3-5 for detection <br />limits of motor vehicle fuels (gasoline and diesel). Refer to 1.2-3 "Regional Board Staff Recommendations for Initial <br />Tvaluntion and Investigation of UST's" for the waste and motor oil detection limits. <br />I)eterti„n Limits that remnin below the MCL, STLC or Allowable Limit or the contaminant In question will be accepted, <br />however Inhoratory shall utilize the most conservative method. <br />LAIFOILA'T'ORY ANALYSTS TERMINOLOGY: <br />TPI lG <br />Total Petroleum Hydrocarbon, Gasoline, GCMD (5030) 8015 mod or GUMS 8260 <br />I M-111 <br />Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260 <br />R IX 1�1 F <br />Benzene, Toluene, Xylene & Ethyl Benzene, GC/PID 8020 or GCIMS 8260 <br />CI. I LC <br />Chlorinated I fydrocarbon, GC/HSD 8010, OC/lAS 8240 <br />I'M 'AI. LEAD <br />'Total lead, AA 7420, AA 7421 or ICP -AES 6010 <br />Fl )R <br />Ethvlene dibromide (DHS -AB 1803), GUMS 8240 (DHS -Luft) <br />Gt Tin <br />Gas Chromatography, Flame Ionization Detection <br />ICAP or AA <br />inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel. <br />PC 11 <br />Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br />Niel hod ,050 <br />Acid digestion <br />Mcihod 1540 <br />Soshlct Sample preparation <br />Method 1SSO <br />Sonication snmple preparation, extraction method <br />Method 5010 <br />Purge and trap sample preparation <br />Q,t'Qt' <br />Quality Assurance/Quality Control <br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns arc <br />preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br />ha�o h, en aril proper QA/AC is followed. <br />For Dl inking water sources, FTA recommends that the 500 series for volatile organics be used in preference to the 600 scrie, <br />hecmus• IIIc detection iinim ure lower the Q/VQC 19 better. <br />F11 2: 048 (Rev 2/8/91) Page 8 <br />