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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-0100 Fu(209)668-9516 <br /> email: Iab.geoQatt.net <br /> Report# W012808 Project: John Deer/Sierra Chemical,Stockton CA Date:09/30/10 <br /> San Joaquin County Environmental Health Date Rec'd:09/28/10 <br /> 600 East Main Street <br /> Stockton.CA 95202 <br /> Inorganic Chemistry - Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> ,anal is Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch W002571 -3010A Prepared&Analyzed: 09/28/10 <br /> Matrix Spike Dup(W002.571-MSD1) Source:W012112-01 <br /> Antimony 23.0 1.0 ug/L 25.00 ND 92 80-120 8 20 <br /> Arsenic 34.0 2.00 25.00 8.40 102 80-120 11 20 <br /> Barium 123 20.0 62.50 52.0 114 80-120 0 20 <br /> Beryllium 23.0 0.1 25.00 ND 92 80-120 0 20 <br /> Cadmium 23.0 0.1 25.00 ND 92 80-120 0 20 <br /> Chromium 26.0 1.00 25.00 3.60 90 80-120 4 20 <br /> Cobalt 23.0 1.00 25.00 ND 92 80-120 4 20 <br /> Copper 24.0 1.00 25.00 3.50 82 80.120 4 20 <br /> Lead 27.0 1.00 25.00 ND 108 80-120 4 20 <br /> Mercury 5.70 1.00 6.250 ND 91 80-120 2 20 <br /> Molybdenum 33.0 10.0 25.00 5.4 110 80-120 3 20 <br /> Nickel 27.0 1.0 " 24.00 6.5 82 80-120 0 20 <br /> Selenium 22.0 1.0 25.00 2.0 80 80.120 0 20 <br /> Silver 31.0 2.0 25.00 1.4 118 80-120 0 20 <br /> Thallium 26.0 1.0 25.00 ND 104 80-120 0 20 <br /> Vanadium 49.0 10.0 25.00 30.0 76 80-120 4 20 QM-01 <br /> Zinc 50.0 1.0 25.OD 29.0 84 80-120 2 20 <br /> Batch W002605.3050B Prepared &Analyzed: 09/29/10 <br /> Blank(W002605-BLKI) <br /> Antimony ND 0.5 mg/kg <br /> Arsenic ND 0.5 " <br /> Barium NO, 0.5 " <br /> Beryllium ND 0.5 " <br /> Cadmium ND 06 ' <br /> Chromium ND 0.5 " <br /> Cobalt ND 0.5 " <br /> Copper ND 0.5 " <br /> Lead ND 1.0 " <br /> Molybdenum ND 0.5 " <br /> Nickel ND 0.5 " <br /> Selenium ND 0.5 " <br /> Silver ND 1.0 " <br /> Thallium ND 0.5 " <br /> Vanadium ND 0.5 " <br /> Zinc ND 0.5 " <br /> Mercury ND 0.5 " <br /> Certification#2585 <br />