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J <br /> Analytical Data <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Client Sample ID: B-S(1') <br /> Lab Sample ID: 720-22819-8 Date Sampled: 09124/20091015 <br /> Client Matrix: Solid Date Received:09/24/2009 1900 <br /> 82608 Volatile Organic Compounds(GC/MS) <br /> Method 8260B Analysis Batch:720.58549 Instrument ID: HP12 <br /> Preparation: 50308 Prep Batch:720-58736 Lab File ID: 09290912.D <br /> Dilution: 1.0 Initial Weight/Volume: 5.13 g <br /> Dale Analyzed: 09/29/2009 1356 Final WeighiNolume: 10 mL <br /> Date Prepared: 09/29/2009 0800 <br /> Analyte DryVN Corrected:N Result(ug/Kg) Qualifier RL <br /> N-Propylbenzene NO 4.9 <br /> Styrene NO 4.9 <br /> 1,1,1,2-Tetrachloroethane ND 4.9 <br /> 1,1.22-Tetrachloroethane ND 4.9 <br /> Tetrachloroethene ND 4.9 <br /> Toluene ND 4.9 <br /> 1,2.3-Trichlorobenzene ND 4.9 <br /> 12,4-Trichlorobenzene NO 4.9 <br /> 1,1,1-Tnchloroethane NO 4.9 <br /> 1,1,2-Tnchloroethane NO 4.9 <br /> Trichloroethene NO 4.9 <br /> Trichlorofluoromethane NO 4.9 <br /> 1,2.3-Trichloropropane NO 4.9 <br /> 1,1,2-Tnchloro-1,2,2-trifluoroelhane NO 4.9 <br /> 1,2,4-Tdmethylbenzene NO 4.9 <br /> 1,3,5-Tri methylbenzene NO 4.9 <br /> Vinyl acetate NO 49 <br /> Vinyl chloride NO 4.9 <br /> Xylenes,Total NO 9.7 <br /> 2,2-Dichloropropane NO 4.9 <br /> Surrogate %Rec Qualifier Acceptance Limits <br /> 4-Bromofluorobenzene 91 52-130 <br /> 1,2-Dichloroethane-d4(Sum) 109 67-132 <br /> Toluene-d8(Sum) 100 58-130 <br /> TestAmerica San Francisco Page 24 of 102 10/13/2009 <br />